Hydrogen containing industrial waste gas separation and purification method
A technology for industrial waste gas and hydrogen, applied in separation methods, chemical instruments and methods, hydrogen separation, etc., can solve the problems of hydrogen separation and pressurization of gas with complex components, no energy saving, large limitations, etc., and achieve short process, The effect of less land occupation and great development potential
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Embodiment 1
[0042] Composition is H 2 70%, N 2 23%, (Ar+CH 4 ) 7% mixed gas is first humidified in 85°C hot water through a gas humidifier, and then directly passed into the electrochemical hydrogen pump battery, that is, the gas separation battery. The battery bipolar plate flow used in this battery Field such as Figure 4 Shown (the positive electrode flow field, the negative electrode flow field and the positive electrode flow field are mirror symmetric); the proton exchange membrane used in this battery is a perfluorosulfonic acid membrane with a thickness of 50 μm; the positive electrode catalyst used in this battery is platinum, Loading capacity 0.35mg / cm 2 , the negative electrode catalyst is platinum, and the loading capacity is 0.3mg / cm 2 . The voltage applied to the battery is 0.3V, and the current density is 300mA / cm 2 . The temperature of the battery is kept at 80±2.5°C, the pressure of the battery positive air chamber is 0.20MPa, the pressure of the negative air cham...
Embodiment 2
[0044] The mixed gas (pressure is 0.20MPa) with the same composition as in Example 1 is first humidified in 85°C hot water by a gas humidifier, and then directly passed into a battery pack in series consisting of 3 electrochemical hydrogen pump cells The first battery in the battery, the exhaust gas comes out from the positive electrode of the first battery, is separated to remove moisture, and is discharged. The pure hydrogen gas from the negative electrode of the first battery enters the positive electrode of the second battery, and under the action of an external electric field, the hydrogen gas "permeates" into the negative electrode of the second battery, and the gas pressure increases to 0.30MPa. The hydrogen gas from the negative electrode of the second battery continues to be pressurized in the third battery to reach 0.35MPa. The battery bipolar plate flow field used in the battery of this gas separation battery pack is as follows Figure 4 Shown (the positive electro...
Embodiment 3
[0047] Composition is H 2 50%, CO 2 15%, CH 4 6%, (Ar+N 2 )29%, CO content about 5ppm, H 2 A mixed gas with an S content of about 1.4ppm (at a pressure of 0.25MPa) is directly passed into the first battery in a series battery pack consisting of three electrochemical hydrogen pump batteries, and the exhaust gas is discharged from the positive electrode of the first battery. Come out, separate to remove water, discharge. The pure hydrogen gas from the negative electrode of the first battery enters the positive electrode of the second battery. Under the action of an external electric field, the hydrogen gas "permeates" into the negative electrode of the second battery, and the gas pressure increases to 0.35MPa. The hydrogen gas from the negative electrode of the second battery continues to be pressurized in the third battery to reach 0.40MPa. The battery bipolar plate flow field used in the battery of this gas separation battery pack is as follows Figure 4 Shown (the po...
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