Eastern larch bark rapid pyrolysis oil modified phenolic resin adhesive
A technology for pyrolysis of oil and larch, applied in the direction of adhesives, aldehyde/ketone condensation polymer adhesives, adhesive types, etc., can solve the problems of reducing reaction temperature, excessive average molecular weight, and reducing free formaldehyde content, etc. Achieve the effect of low formaldehyde emission and low cost
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[0016] The invention provides a kind of preparation method of pyrolysis oil modified PF resin, specific example is as follows:
example 1
[0017] Example one: pyrolysis oil and phenol weight ratio are 40%, formaldehyde: phenol-pyrolysis oil mixture (mixture molecular weight is considered to be identical with phenol): the molar ratio of NaOH 1.8: 1: 0.4, add water and make system solid content reach 50%. Put the measured phenol, sodium hydroxide (4 / 5) and water into the reaction kettle at the same time, stir for 10 minutes, raise the internal temperature to 40-42°C, add a part of formaldehyde, raise the temperature to 80-85°C within 45min, keep warm After 20 minutes, heat the reactant to 90-95°C within 10 minutes, keep it in this state for 15 minutes, cool down to 75°C, add the remaining formaldehyde, the remaining sodium hydroxide and pyrolysis oil, heat to 78-80°C, and react When the viscosity is qualified (400-800cp), cool down to 40°C and discharge.
example 2
[0018] Example two: the weight ratio of pyrolysis oil and phenol is 40%, formaldehyde: phenol-pyrolysis oil mixture (mixture molecular weight is considered to be identical with phenol): the molar ratio of NaOH is 1.8: 1: 0.35, and water is added to make the system contain 50% solid. Put the measured phenol, sodium hydroxide (4 / 5) and water into the reaction kettle at the same time, stir for 10 minutes, raise the internal temperature to 40-42°C, add a part of formaldehyde, raise the temperature to 80-85°C within 45min, keep warm After 20 minutes, heat the reactant to 90-95°C within 10 minutes, keep it in this state for 15 minutes, cool down to 75°C, add the remaining formaldehyde, the remaining sodium hydroxide and pyrolysis oil, heat to 80-85°C, and react When the viscosity is qualified (400-800cp), cool down to 40°C and discharge.
[0019] indicators
Traditional PF resin
PF resin with 40% replacement rate of larch bark pyrolysis oil
Solid content
...
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