Expansion flame-proof organosilicon fluid sealant and method of producing the same
A technology of intumescent flame retardant and intumescent flame retardant, which is applied in the field of flame retardant materials, can solve problems such as ship sinking and threat to ship safety, and achieve the effects of ensuring personnel and property safety, good fire resistance and convenient construction.
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[0035] Example 1
[0036] Combine 90 parts of α,ω-dihydroxypolydimethylsiloxane with a viscosity of 100,000mPa·s, 10 parts of α,ω-dihydroxypolydimethylsiloxane with a viscosity of 500mPa·s, and 30 parts of colloidal calcium carbonate , 40 parts of aluminum hydroxide, 20 parts of basic zinc carbonate, 15 parts of amine polyphosphate into the vacuum planetary mixer at a temperature of 80 ℃, vacuum degree -0.06 ~ -0.095MPa, dehydration and blending for 1 hour; cooling to room temperature, 8 parts of methyl trimethoxy silane, 1 part of γ-aminopropyl triethoxy silane, 0.2 parts of dibutyl tin dilaurate, 10 parts of dimethicone, α, ω-dimethoxy polydimethyl Add 10 parts of base siloxane and 5 parts of inorganic pigment iron oxide red into the vacuum planetary mixer, the vacuum degree is -0.06~-0.095MPa, and blend for 1.5 hours to obtain intumescent flame-retardant silicone sealant. The performance of the product in different states The test structure is shown in Table 1.
Example Embodiment
[0037] Example 2
[0038] Combine 100 parts of α,ω-dihydroxy polydiethylsiloxane with a viscosity of 50,000 mPa·s, 10 parts of fumed white carbon black, 20 parts of kaolin, 80 parts of magnesium hydroxide, 20 parts of zinc borate, and 20 parts of expanded graphite. Add parts to a vacuum planetary mixer at a temperature of 100°C, a vacuum degree of -0.06~-0.095MPa, dehydration and blend for 1 hour; cool to room temperature, add 14 parts of methyltriethoxysilane, γ-aminopropyltrimethoxy Add 2 parts of silane, 0.6 parts of butyl titanate, 10 parts of branched silicone oil, and 0.5 parts of inorganic pigment carbon black into the vacuum planetary mixer, the vacuum degree is -0.06~-0.095MPa, and blend for 2 hours to obtain the intumescent flame retardant organic For silicon sealant, the performance test structure of the product in different states is shown in Table 1.
Example Embodiment
[0039] Example 3
[0040] Combine 60 parts of α,ω-dihydroxypolydimethylsiloxane with a viscosity of 50,000mPa·s, 40 parts of α,ω-dihydroxypolydimethylsiloxane with a viscosity of 2000mPa·s, and 40 parts of colloidal calcium carbonate. Part, 20 parts of quartz powder, 80 parts of magnesium hydroxide, 20 parts of basic zinc carbonate, 25 parts of expanded graphite are put into a vacuum planetary mixer at a temperature of 120°C, a vacuum degree of -0.06~-0.095MPa, dehydration and blending for 1.5 hours; Cool to room temperature, add 18 parts of methyl ketoxime silane, 2 parts of γ-aminopropyl trimethoxysilane, 0.5 parts of isobutyl titanate, 8 parts of dimethyl silicone oil, and 3 parts of inorganic pigment iron oxide blue. In the vacuum planetary mixer, the vacuum degree is -0.06~-0.095MPa, and the blending is 1.5 hours to obtain the intumescent flame-retardant silicone sealant. The performance test structure of the product in different states is shown in Table 1.
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