Method for preparing low-oxygen aluminum nitride powder by auto-igniting synthesis
A low oxygen content, self-propagating combustion technology, applied in chemical instruments and methods, nitrogen compounds, inorganic chemistry, etc., can solve the problems of incapable of large-scale production process, high oxygen content and complexity of powder, and achieve rapid synthesis reaction time , high purity and narrow particle size distribution
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[0032] In Example 1, a metal aluminum powder with a particle size of 300 mesh (purity of metal aluminum powder> 99.5%, iron content 98.8%) 50%, NH4 After mixing Cl5wt%, put it into the pot mill. The pot mill is lined with polyurethane and Al 2 O 3 The ball is the ball milling medium, the weight ratio of material: ball is 1:4, and the ball is milled for 2 hours. The powder after ball milling is passed through a 40-mesh screen. The sieved material is evenly placed in a porous semi-cylindrical graphite boat, and then leveled. Put it into the spontaneous combustion synthesis reactor, after evacuating, fill with high-purity nitrogen to 2MPa, and then exhaust. This process is repeated 3 times, then fill with high-purity nitrogen until the pressure is maintained at 3MPa, and use a tungsten wire with a diameter of 0.6mm. The heating element is fed with a current of 25 amperes. The ignition time lasts for 15 seconds. The ignition induces the spontaneous combustion reaction of the raw mater...
Example Embodiment
[0033] In Example 2, metal aluminum powder with a particle size of 200 mesh (purity of metal aluminum powder> 99.5%, iron content 4 Cl 15wt%, sodium azide 5wt% are mixed and put into the three-dimensional motion mixer. The mixer is lined with polyurethane and Al 2 O 3 The ball is a ball milling medium, the weight ratio of material: ball is 1:8, and the ball is milled for 5 hours. The powder after ball milling is passed through a 40-mesh screen. The sieved material is evenly placed in a porous semi-cylindrical graphite boat, and then leveled. Put it into the spontaneous combustion synthesis reactor, after vacuuming, fill with high-purity nitrogen to 2MPa, and then exhaust. This process is repeated 3 times, then fill with high-purity nitrogen until the pressure is kept at 4.5MPa, and use nickel-chromium with a diameter of 0.6mm The wire is used as a heating element, and an electric current of 25 amperes is passed through. The ignition induces the spontaneous combustion reaction of t...
Example Embodiment
[0034] In Example 3, metal aluminum powder with a particle size of 100 mesh (purity of metal aluminum powder> 99.5%, iron content 4 Cl 15wt% and sodium azide 5wt% are mixed and put into the three-dimensional motion mixer. The mixer is lined with polyurethane and Al 2 O 3 The ball is a ball milling medium, the weight ratio of material: ball is 1:6, and the ball is milled for 3 hours. The powder after ball milling is passed through a 40-mesh screen. The sieved material is evenly placed in a porous semi-cylindrical graphite boat, and then leveled. Put it into the spontaneous combustion synthesis reactor, after evacuating, fill with high-purity nitrogen to 2MPa, and then exhaust. This process is repeated 3 times, then fill with high-purity nitrogen until the pressure is maintained at 6MPa, and use a nickel-chromium wire with a diameter of 0.6mm As a heating element, a 25 ampere current is applied to ignite the raw material powder to initiate a spontaneous combustion reaction. During t...
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