Metal nitride electrode material for dye-sensitized solar cell
A technology of solar cells and dye sensitization, which is applied in the field of metal nitride electrode materials for dye-sensitized solar cells, can solve the problems of expensive platinum and high manufacturing costs of electrodes, and achieve small surface resistance, long service life and high stability Effect
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Embodiment 1
[0016] The preparation of embodiment 1 nickel nitride nanoparticle film electrode material, the steps are as follows:
[0017] 1) the nickel oxide nanoparticle slurry is made into a porous film with a thickness of 8 microns by screen printing;
[0018] 2) Put the nickel oxide film in a tube furnace with flowing ammonia gas, and nitriding it for 1 hour at a temperature of 400° C. to 450° C. to prepare a nickel nitride porous electrode material.
[0019] The prepared nickel nitride porous electrode material was used for figure 1 The counter electrode of the dye-sensitized solar cell shown, its photocurrent-voltage curve is measured as figure 2 It is shown that it has good electrochemical performance.
Embodiment 2
[0020] Embodiment 2 The preparation of iron nitride nanoparticle thin film electrode material, the steps are as follows:
[0021] 1) The iron oxide nanoparticle slurry is made into a porous film with a thickness of 18 microns by spraying;
[0022] 2) placing the iron oxide film in a tube furnace with flowing nitrogen gas, and nitriding it for 1 hour at a temperature of 400-450° C. to prepare an iron nitride electrode material.
[0023] The prepared iron nitride electrode material was used for figure 1 The counter electrode of the dye-sensitized solar cell shown, its photocurrent-voltage curve is measured as image 3 It is shown that it has good electrochemical performance.
Embodiment 3
[0024] Embodiment 3 The preparation of cobalt nitride nanoparticle thin film electrode material, the steps are as follows:
[0025] 1) the cobalt oxide nanoparticle slurry is made into a porous film with a thickness of 38 microns by scraping;
[0026] 2) Place the cobalt oxide film in a tube furnace with flowing hydrazine, and nitride it for 1 hour at a temperature of 450° C. to prepare a cobalt nitride porous electrode material.
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Abstract
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