Extraction method of Chinese torreya shell essential oil
An extraction method and a technology for Torreya torreya are applied in the field of extracting essential oil of Torreya husks, which can solve the problems of large consumption of organic solvents, high oil yield, easy residues and the like, and achieve the effects of solving waste utilization, promoting overall upgrading and low cost.
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Embodiment 1
[0025] equipment:
[0026] German KOMET DD85G cold press;
[0027] LXJ-II centrifugal sedimentation machine
[0028] instrument:
[0029] Agilent 7890-5975 GC-MS column model: HP-Innowax 60m×0.25mm×0.25μm
[0030] French Alpha M.O.Sα-FOX4000 electronic nose
[0031] Gas chromatography conditions:
[0032] The initial temperature was maintained at 50°C for 5 minutes, raised to 220°C at 3°C / min, and maintained for 5 minutes. Injection port temperature: 250°C; split ratio 50:1; injection volume 1 μl Chromatographic library: wiley7n and nist05 library.
[0033] Extract essential oil from fresh Torreya husk
[0034] Take 3 kg of fresh Chinese torreya shells, after simple shearing, soak in 5% sodium sulfate solution for 8 hours, drain the water, use a cold press to squeeze the juice from the soaked Chinese torreya shells, and obtain about 6.5 liters of mixed solids liquid, the mixed solution is centrifuged with a centrifugal sedimentation machine, and after separation and pre...
Embodiment 2
[0040] equipment:
[0041] FX type traditional Chinese medicine grinder
[0042] instrument:
[0043] Agilent 7890-5975 GC-MS column model: HP-Innowax 60m×0.25mm×0.25μm
[0044] French Alpha M.O.Sα-FOX4000 electronic nose
[0045] Gas chromatography conditions:
[0046] The initial temperature was maintained at 50°C for 5 minutes, raised to 220°C at 3°C / min, and maintained for 5 minutes. Injection port temperature: 250°C; split ratio 50:1; injection volume 1 μl Chromatographic library: wiley7n and nist05 library.
[0047] Extract essential oil from stale torreya husk
[0048] Take stale torreya shells, put them in a ZK-82A vacuum drying oven at 60°C and dry them after simple grading, until the water content of the torreya shells reaches 5%, and use the FX type traditional Chinese medicine grinder to crush the dried torreya shells to make the torreya shell powder When the number reaches about 80-100 mesh, 3 kg of the obtained powder is distilled by water distillation. Befor...
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