Method for preparing hydroxylapatite coating by microplasma spraying
A hydroxyapatite, microbeam plasma technology, applied in the field of biomedical implant material preparation, can solve the problems of low and low utilization rate of powder, only 20-50%, premature dissolution and peeling, etc. good biological activity
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Embodiment 1
[0013] Embodiment 1: The hydroxyapatite powder is sprayed onto the substrate by using a micro-beam plasma spraying system. The gas flow rate is 1.0L / min, the protective gas is industrial pure argon, the protective gas flow rate is 0.5L / min, the powder feeding gas is industrial pure argon, the powder feeding gas flow rate is 4L / min, the powder feeding rate is 0.05g / min, and the working current is 40A. Gun pendulum speed 150mm / min, stepping 2mm, spraying times 3 times, spraying distance 80mm, the obtained coating thickness is 50μm; powder utilization rate is 90%, crystallinity is 85%.
Embodiment 2
[0014] Example 2: The hydroxyapatite powder is sprayed onto the substrate by using a micro-beam plasma spraying system. The gas flow rate is 1.1L / min, the protective gas is argon-helium mixed gas, the protective gas flow rate is 0.4L / min, the powder feeding gas is argon-helium mixed gas, the powder feeding gas flow rate is 5L / min, the powder feeding rate is 0.10g / min, and the working current 35A, gun swing speed 600mm / min, stepping 3mm, spraying times 2 times, spraying distance 70mm, the coating thickness is 20μm; the powder utilization rate is 74%, and the crystallinity is 79%.
Embodiment 3
[0015] Embodiment 3: The hydroxyapatite powder is sprayed onto the substrate by using a micro-beam plasma spraying system. The gas flow rate is 1.2L / min, the protective gas is argon-helium mixed gas, the protective gas flow rate is 0.4L / min, the powder feeding gas is argon-helium mixed gas, the powder feeding gas flow rate is 5L / min, the powder feeding rate is 0.50g / min, and the working current 60A, gun swing speed 3900mm / min, stepping 2mm, spraying times 3 times, spraying distance 100mm, the coating thickness is 100μm; the powder utilization rate is 70%, and the crystallinity is 65%.
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