Preparation method of highly oriented tube-shaped through hole porous ceramics
A technology of porous ceramics and directional tubes, which is applied in the field of ceramic materials, can solve the problems of no reports, etc., and achieve the effects of simple preparation process, dense hole wall, and high green body strength
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Embodiment 1
[0034]At a temperature of 35°C, mix tert-butanol, PVB, and PEG according to the mass ratio of tert-butanol:PVB:PEG=100:3:3 to prepare a pre-prepared solution, and add submicron Grade alumina powder is ball milled for 6 hours at 25°C to 30°C to obtain a stable ceramic suspension. The ceramic suspension is injected into the mold at 30°C, and then the suspension and the mold are placed on a constant temperature bath. The bottom of the ceramic suspension is at a constant low temperature of -30°C. Except for the bottom of the ceramic suspension in the mold, the rest of the ceramic suspension is in an adiabatic state. , keep the bottom at a constant temperature for 4-8 hours, put the green body that has formed the directional air hole template together with the mold into a low-temperature refrigerator (below -50°C) for 24-72 hours, then take out the mold and the green body, and demould at 0°C , put it into a freeze dryer, dry it in vacuum at -50°C for 24 hours, then heat it up to 50...
Embodiment 2
[0036] At a temperature of 35°C, mix and prepare tert-butanol, PVP, deionized water, and silane coupling agent according to the mass ratio of tert-butanol:PVP:deionized water:silane coupling agent=100:15:8:1 To become a pre-prepared solution, add submicron lead zirconate titanate powder according to the solid phase volume fraction of 25 vol%, and ball mill for 4 hours under the condition of 25° C. to 30° C. to obtain a stable ceramic suspension. The ceramic suspension is injected into the mold at 30°C, and then the suspension and the mold are placed on a constant temperature tank. The bottom of the ceramic suspension is at a constant low temperature of -170°C. Except for the bottom of the ceramic suspension at a constant temperature, the rest of the ceramic suspension in the mold is insulated. , keep the bottom at a constant temperature for 4-8 hours, put the green body that has formed the directional air hole template together with the mold into a low-temperature refrigerator ...
Embodiment 3
[0038] At a temperature of 45°C, tert-butanol and PVB were mixed according to the mass ratio of tert-butanol:PVB=100:5 to form a pre-prepared solution, and submicron zirconia powder was added according to the solid phase volume fraction of 20vol%. Ball mill for 4 hours under the condition of 25°C-30°C to obtain a stable ceramic suspension. The ceramic suspension is injected into the mold at 30°C, and then the suspension and the mold are placed on a constant temperature tank. The bottom of the ceramic suspension is at a constant low temperature of 10°C. Except for the bottom of the ceramic suspension in the mold, the rest is in adiabatic state. Keep the bottom at a constant temperature for 4 to 8 hours, put the green body that has formed the directional air hole template together with the mold into a low-temperature refrigerator (below -50°C) for 24 to 72 hours, then take out the mold and the green body, and demould at 10°C. Put it into a freeze dryer, dry it in vacuum at -50°C...
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