Method for preparing cobaltosic oxide by calcinating cobalt oxalate with microwave
A technology of cobalt tetroxide and cobalt oxalate, applied in the direction of cobalt oxide/cobalt hydroxide, etc., can solve the problems of uneven product composition and particle size, high production cost, complex equipment structure, etc., and achieve uniform product composition and particle size, suitable for industrial production, Solve the effect of high energy consumption
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Embodiment 1
[0018] Example 1: Cobalt oxalate with a particle size of 100-250 μm obtained through crystallization and precipitation during the cobalt wet extraction process was dried until the water content was less than 5 wt%, and placed in the microwave rotary kiln silo, and the feed screw speed was adjusted to 3 rpm. The material is continuously conveyed to the composite microwave heating tube of the microwave rotary kiln with an inclination angle of 5° through the feeding screw, the microwave heating switch is turned on, the microwave output power is adjusted to 10-15kW, the rotary kiln speed is adjusted to 2 rpm, and the silicon carbide section The material is heated from room temperature to 500-530°C at a rate of 20°C / min, so that the partially decomposed material in the silicon carbide section is transported to the microwave-specific ceramic section with axial rib diameter, and the residence time of the material in the rotary kiln is controlled as After 35 minutes, the cobalt tetraox...
Embodiment 2
[0019] Example 2: The feed screw speed is 6 rpm, the microwave output power is adjusted to 40-45kW, the temperature of the silicon carbide section material is raised from room temperature to 530-560 °C at a rate of 50 °C / min, and the rotary kiln speed is adjusted to 5 rpm , so that the partially decomposed material in the silicon carbide section is transported to the special microwave ceramic section with axial rib diameter, and the residence time of the material in the rotary kiln is controlled to be 20 minutes. After being fully reacted by the microwave special ceramic section, it enters the recovery system, and the Cobalt Tetroxide Products. After analysis and testing, the cobalt content in the tricobalt tetroxide product is 73.0%, and the average particle size is 3-8 μm.
Embodiment 3
[0020] Example 3: The feed screw speed is 9 rpm, the microwave output power is adjusted to 70-75kW, the temperature of the silicon carbide section material is raised from room temperature to 560-600 °C at a rate of 80 °C / min, and the rotary kiln speed is 8 rpm, The material that has been partially decomposed in the silicon carbide section is transported to the special microwave ceramic section with axial rib diameter, and the residence time of the material in the rotary kiln is controlled to be 10 minutes. product. After analysis and testing, the cobalt content in the tricobalt tetroxide product is 72.8%, and the average particle size is 1-7 μm.
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