Niobium tungstate compound for resisting hepatitis virus
A niobium tungstate compound, hepatitis technology, applied in the field of niobium tungstate compound against hepatitis virus
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Embodiment 1
[0059] Anti-hepatitis virus niobium tungstate compound Na 7 [Ge(NbO 2 ) 3 W 9 o 37 ]·15H 2 Preparation of O.
[0060] a. Dissolve 3.9g of sodium hydroxide in a nickel crucible, dissolve at 350°C, and slowly add 3.3g of Nb 2 o 5 , heated for 30 minutes, then cooled to room temperature, added to 50mL of deionized water, and left at 0°C for 12 hours to generate needle-like crystal products, and the hexaniobate compound Na7H[Nb 6 o 19 ];
[0061] b. Dissolve 11g of sodium germanate in 250mL of distilled water, and add 100g of sodium tungstate dihydrate while stirring. Slowly add 6mol / L concentrated hydrochloric acid solution to adjust the pH value of the solution to 8-9, a small amount of white precipitate is produced, the precipitate is suction filtered, and the filtrate is placed at 4°C for 2-3 days to obtain a white needle-shaped crystal vacancy heteropoly compound Na 9 H[GeW 9 o 34 ], wash the crystals with cold water, ethanol, ether for later use;
[0062] c. the 8...
Embodiment 2
[0064] Anti-hepatitis virus niobium tungstate compound K 7 [Si(NbO 2 ) 3 W 9 o 37 ]·14.5H 2 Preparation of O.
[0065] a. Dissolve 5.5g of potassium hydroxide in a nickel crucible, dissolve at 320°C, and slowly add 3.3g of Nb 2 o 5 , heated for 30 minutes, then cooled to room temperature, added to 50 mL of deionized water, and left at 0°C for 12 hours to form a needle-like crystal product and obtain hexaniobate compound K 7 H[Nb 6 o 19 ];
[0066] b. Dissolve 12g of sodium silicate in 250mL of distilled water, add 150g of sodium tungstate dihydrate while stirring, slowly add 6mol / L concentrated hydrochloric acid solution to adjust the pH value of the solution to 8.2, a small amount of white precipitate is produced, and the precipitate is suction filtered, and the filtrate Placed at 4°C for 2-3 days, a white needle-like crystal vacancy type heteropoly compound Na appears 9 H[SiW 9 o 34 ], wash the crystals with cold water, ethanol, ether for later use;
[0067] c....
Embodiment 3
[0069] Anti-hepatitis virus niobium tungstate compound Cs 6 H[Si(NbO 2 ) 3 W 9 o 37 ]·2H 2 Preparation of O.
[0070] a. same as embodiment 2 step a, make hexaniobate compound K 7 H[Nb 6 o 19 ];
[0071] b. same as Example 2, step b, to prepare the vacancy type heteropoly compound Na 9 H[SiW 9 o 34 ];
[0072] c. the 6.5g K obtained in step a 7 H[Nb 6 o 19 ] was dissolved in 400mL deionized water, then 40mL hydrogen peroxide was added in this niobate aqueous solution, acidified with about 20mL of 3mol / L hydrochloric acid, and then 25.1g of Na 9 H[SiW 9 o 34 ] into the niobate solution, dilute to 700mL with water, stir gradually to form a clear, dark yellow solution, add 10g of CsCl precipitant, evaporate the solution to 350mL at room temperature, filter, and wash with distilled water at 4°C to obtain a yellow solid Cs 6 H[Si(NbO 2 ) 3 W 9 o 37 ]·2H 2 O.
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