Method for preparing high-performance iron nickel magnetically soft alloy by using powder metallurgy process

A powder metallurgy and soft magnetic alloy technology, applied in the field of powder metallurgy, can solve problems such as material shortage, and achieve the effects of reducing impurity content, improving microstructure and structure, and increasing density

Active Publication Date: 2010-11-17
UNIV OF SCI & TECH BEIJING
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, when powder metallurgy is used to prepare iron-nickel soft magnetic alloys, the magnetic permeability of the prepared soft magnetic alloys is far lower than that of soft magnetic alloys prepared by smelting process due to the shortage of materials in t

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0014] Iron powder and nickel powder are selected as raw material powders, and the ratio of iron powder: nickel powder is 50:50 by weight percentage, and then ball milled and mixed in a ball mill for 180 minutes. The mixed powder is pressed into shape, and the shaped blank is kept at 1320°C for 600 minutes under vacuum conditions, and then subjected to hot isostatic pressing at 1100°C and 150 MPa for 180 minutes. The hot isostatic pressed product is treated under vacuum conditions at 1200°C for 300 minutes to obtain a high-performance iron-nickel soft magnetic alloy product.

Embodiment 2

[0016] Iron powder and nickel powder are selected as raw material powders, and the ratio of iron powder: nickel powder is 50:50 by weight percentage, and then ball milled and mixed in a ball mill for 180 minutes. The mixed powder is pressed into shape, and the formed blank is kept at 1360°C and 0.5MPa for 120 minutes, and then hot isostatically pressed at 1200°C and 150MPa for 180 minutes. The hot isostatic pressed product is treated under vacuum conditions at 1300°C for 600 minutes to obtain a high-performance iron-nickel soft magnetic alloy product.

Embodiment 3

[0018] Iron powder and nickel powder are selected as raw material powders, and the ratio of iron powder: nickel powder is 50:50 by weight percentage, and then ball milled and mixed in a ball mill for 240 minutes. The mixed powder is pressed into shape, and the molded blank is kept at 1380°C and 1MPa for 300 minutes, and then hot isostatically pressed at 1150°C and 150MPa for 180 minutes. The hot isostatic pressed product is treated under the conditions of 1360°C and 1MPa for 600 minutes to obtain a high-performance iron-nickel soft magnetic alloy product.

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Abstract

The invention discloses a method for preparing high-performance iron nickel magnetically soft alloy by using a powder metallurgy process, which belongs to the technical field of powder metallurgy. The method comprises the following steps of: 1, uniformly mixing various powder such as iron powder, nickel powder, molybdenum powder, silicon powder, copper powder, cobalt powder, chrome powder, niobium powder, tungsten powder, aluminum powder and titanium powder according to a certain ratio, wherein the nickel content ranges from 30 to 78 percent; or the alloy powder prepared according to a certain alloy component ratio is directly used as a raw material; 2, forming the powder which is obtained by step 1 into a blank with a certain shape by using a powder metallurgy forming method; 3, sintering the formed blank, which is obtained by the step 2, under the pressure of between 0 and 1,000 MPa and at the temperature of between 600 and 1,500 DEG C for 10 to 4,000 minutes; and 4, processing the sintered body obtained by the step 3 under the pressure of between 0 and 4,000 MPa and at the temperature of between 600 and 1,600 DEG C for 0 and 4,000 minutes. The method has the characteristic that: by improving the sintering and thermal treatment systems, the material density is improved, the micro texture and structure of the material are improved, the impurity content is reduced, and the magnetically soft alloy product with the maximal magnetic conductivity of no less than 40 mH/m and with the coercive force of no more than 20 A/m can be prepared.

Description

technical field [0001] The invention belongs to the field of powder metallurgy, and in particular provides a method for preparing a high-performance iron-nickel system soft magnetic alloy by adopting a powder metallurgy process. Background technique [0002] The iron-nickel soft magnetic alloy with a nickel content of 30%-90% is a soft magnetic material with excellent comprehensive magnetic properties, and it is also one of the most representative alloys in soft magnetic materials. It is famous for its high magnetic permeability and low coercive force, and its application is also very extensive, especially as a magnetic conductive component, it has become an indispensable basic material for communication, radar, aerospace, computer technology, and precision instrumentation industries. With the development of magnetic circuit components towards miniaturization and multi-function, the size of the soft magnetic alloy parts used is getting smaller and smaller, and the shape is m...

Claims

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Application Information

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IPC IPC(8): C22C19/03C22C38/08C22C1/04C22C33/02H01F1/22
Inventor 曲选辉秦明礼麻季冬王旭张深根田建军刘章文
Owner UNIV OF SCI & TECH BEIJING
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