Method for preparing SiO2/TiO2 composite powder
A composite powder and volume technology, applied in the field of nanomaterials, can solve the problems of difficult separation and control of products, easy agglomeration and growth of primary particles, and high cost, and achieve the effects of shortening the preparation cycle, shortening the process time, and complete the shape
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0026] A SiO 2 / TiO 2 The preparation method of composite powder comprises the following steps:
[0027] 1) Dissolve 10ml tetraethyl orthosilicate in 120ml (part a) of absolute ethanol to form solution A, and dissolve ammonia water (volume concentration 25%) twice the volume of tetraethyl orthosilicate in 80ml (part b) of Dehydrated alcohol is configured into solution B, in terms of mass ratio, tetraethyl orthosilicate / (a+b part of dehydrated alcohol+ammonia)=5:96;
[0028] Put solution A in the ultrasonic equipment, set the power to 100W, the frequency to 40KHz, and the temperature to 30°C, add solution B to solution A under ultrasonication, and then continue ultrasonication for 1h; after the ultrasonication is completed, separate and mix The precipitate generated in the solution, the precipitate was washed with water and absolute ethanol, and then dried at 60°C to obtain SiO with a particle size of 100-400nm 2 submicron spheres;
[0029] 2) Dissolve 192.14g (1mol) of cit...
Embodiment 2
[0034] A SiO 2 / TiO 2 The preparation method of composite powder comprises the following steps:
[0035] 1) Dissolve 10ml tetraethyl orthosilicate in 145ml (part a) of absolute ethanol to form solution A, and dissolve ammonia (volume concentration 28%) that is 8 times the volume of tetraethyl orthosilicate in 112ml (part b) of Dehydrated alcohol is configured into solution B, in terms of mass ratio, tetraethyl orthosilicate / (a+b part of dehydrated alcohol+ammonia)=3:90;
[0036] Put solution A in the ultrasonic equipment, set the power to 80W, set the temperature to 40°C, and set the frequency to 30KHz, add solution B to solution A under ultrasonication, and then continue ultrasonication for 2h; after the ultrasonication is completed, separate and mix The precipitate generated in the solution was washed with water and absolute ethanol and dried at 80°C to obtain SiO 2 submicron spheres;
[0037]2) Dissolve 192.14g (1mol) of citric acid in 300ml of ammonia water with a volu...
Embodiment 3
[0041] A SiO 2 / TiO 2 The preparation method of composite powder comprises the following steps:
[0042] 1) Dissolve 10ml tetraethyl orthosilicate in 120ml (part a) of absolute ethanol to form solution A, and dissolve 6 times the volume of tetraethyl orthosilicate in ammonia (volume concentration 25%) in 120ml (part b) of Dehydrated alcohol is configured into solution B, in terms of mass ratio, tetraethyl orthosilicate / (dehydrated alcohol+ammonia water of a+b part)=3.5:93;
[0043] Put solution A in the ultrasonic equipment, set the power to 85W, set the temperature to 38°C, and set the frequency to 35KHz, add solution B to solution A under ultrasonication, and then continue ultrasonication for 1h; after the ultrasonication is completed, separate and mix The precipitate formed in the solution was washed with water and absolute ethanol and dried at 70°C to obtain SiO 2 submicron spheres;
[0044] 2) Dissolve 192.14g (1mol) of citric acid in 300ml of ammonia water with a vol...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com