Titanium electrode for chlorine generator and preparation method thereof
A technology of chlorine generator and titanium electrode, which is applied in the field of titanium electrode and its preparation, can solve the problems of high chlorine analysis potential and excessive oxygen, and achieve the effect of increasing service life and improving chlorine production efficiency
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Embodiment 1
[0019] 1) Sandblasting the surface of a 0.8 mm thick titanium plate with a required area, then removing the oil stains on the surface with acetone, heating and boiling with 5% oxalic acid solution for 4 hours, then taking it out and soaking it in distilled water for later use.
[0020] 2) Weigh 0.0g of chloroplatinic acid, 2.5g of chloroiridic acid and 7.5g of ruthenium trichloride in a 250ml beaker, add 150ml of isopropanol, and then add 25ml of 37.5% concentrated hydrochloric acid;
[0021] 3) Put the solution obtained in step 2) in ice water, stir well to dissolve the solute completely, then brush it on the surface of the treated titanium plate, dry it at room temperature, and then put it in an oven at 120°C for 3 minutes, then place it in the Bake in a muffle furnace at 500°C for 5 minutes;
[0022] 4) Repeat the steps of brushing, drying, baking, and baking in step 3) 30 times to obtain the titanium electrode sample 1 for the chlorine generator of the present invention. ...
Embodiment 2
[0024] 1) Sandblasting the surface of a 0.8 mm thick titanium plate with a required area, then removing the oil stains on the surface with acetone, heating and boiling with 5% oxalic acid solution for 4 hours, then taking it out and soaking it in distilled water for later use.
[0025] 2) Weigh 1.0g of chloroplatinic acid, 2.25g of chloroiridic acid and 6.75g of ruthenium trichloride in a 250ml beaker, add 150ml of isopropanol, and then add 25ml of 37.5% concentrated hydrochloric acid;
[0026] 3) Put the solution obtained in step 2) in ice water, stir well to dissolve the solute completely, then brush it on the surface of the treated titanium plate, dry it at room temperature, and then put it in an oven at 120°C for 3 minutes, then place it in the Bake in a muffle furnace at 500°C for 5 minutes;
[0027] 4) Repeat the steps of brushing, drying, baking, and baking in step 3) 30 times to obtain the titanium electrode sample 2 for the chlorine generator of the present invention....
Embodiment 3
[0029] 1) Sandblasting the surface of a 0.8 mm thick titanium plate with a required area, then removing the oil stains on the surface with acetone, heating and boiling with 5% oxalic acid solution for 4 hours, then taking it out and soaking it in distilled water for later use.
[0030] 2) Weigh 3.0g of chloroplatinic acid, 1.75g of chloroiridic acid and 5.25g of ruthenium trichloride in a 250ml beaker, add 150ml of isopropanol, and then add 25ml of 37.5% concentrated hydrochloric acid;
[0031] 3) Put the solution obtained in step 2) in ice water, stir well to dissolve the solute completely, then brush it on the surface of the treated titanium plate, dry it at room temperature, and then put it in an oven at 120°C for 3 minutes, then place it in the Bake in a muffle furnace at 500°C for 5 minutes;
[0032] 4) Repeat the steps of brushing, drying, baking and baking in step 3) 30 times to obtain the titanium electrode sample 3 for chlorine generator of the present invention.
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