Transparent dielectric paste
A transparent medium and paste technology, applied in the field of dye-sensitized solar cells, to achieve the effect of strong acid and alkali corrosion resistance and high light transmittance
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[0049] Preparation of III transparent medium slurry
[0050] Weigh the inorganic glass powder according to the proportion and put it in the mixing tank, add the corresponding organic carrier, disperse and mix it on the high-speed shear dispersion equipment, and then pass the mixed slurry through the three-axis rolling mill to further promote the inorganic Dispersion of the glass powder and its fusion with the organic carrier until the fineness of the inorganic glass powder in the slurry is less than 5 μm, and the resulting slurry is filtered through a filter and vacuum defoamed to obtain a transparent medium slurry.
Embodiment 1
[0052] The preparation of I inorganic glass powder:
[0053] According to the following formula (mass percentage): 34% of PbO, 25% of B 2 o 3 , 16% SiO 2 , 18% K 2 O, 7% BeO, weigh each oxide and the corresponding carbonate such as K 2 CO 3 or boric acid.
[0054] After mixing evenly, heat it in a high-temperature solid-phase sintering furnace at 1200°C for 1 hour to obtain uniform molten glass. Pour the molten glass into a double-roll tablet press to cool it rapidly and press it into glass fragments with a thickness of about 1mm. Put the glass fragments into a ball mill jar and coarsely pulverize them on the ball mill until the particles of the glass powder are less than 1mm. The glass powder is milled in a planetary ball mill for more than 24 hours until the particle size specification D90<5 μm (D90: represents the particle size corresponding to 90% of the particle size distribution), and the inorganic glass powder for preparing the slurry is obtained.
[0055] Cast a...
Embodiment 2
[0062] The preparation of I inorganic glass powder:
[0063] According to the following formula (mass percentage): 41% PbO, 25% B 2 o 3 , 23% SiO 2 , 7.5% K 2 O, 3.5% BeO. Weigh each oxide and the corresponding carbonate such as K 2 CO 3 or boric acid H 3 BO 3 After mixing evenly, heat it in a high-temperature solid-phase sintering furnace at 1000°C for 0.5 hours to obtain a uniform molten glass; pour the molten glass into a double-roll tablet press to cool it rapidly and press it into glass fragments with a thickness of about 1mm. Coarsely pulverize the glass powder on a ball mill until the particle size of the glass powder is less than 1mm, and then ball mill the glass powder in a planetary ball mill until the particle size specification D90<10 μm (D90: represents 90% of the particle size distribution. Corresponding particle size), obtain the inorganic glass powder that is used for preparing slurry.
[0064] Preparation of II organic carrier:
[0065] Weigh (meth)a...
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