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Aluminum-magnesium light castable and preparation method thereof

A lightweight castable, aluminum-magnesium technology, applied in the field of castables, can solve the problems of weakening the slag penetration and erosion resistance of materials, limiting the use temperature of aluminum-magnesium materials, and high porosity of porous ceramic particles, so as to achieve thermal shock stability Good, low silicon content, high porosity effect

Active Publication Date: 2013-06-05
WUHAN UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the porous ceramic particles used in the material mentioned above have high porosity, and the average pore size is still relatively large (<30μm). Energy saving needs to be at the expense of weakening the anti-slag penetration and erosion performance of the material, and the lightweight castable is used for a long time. In the parts that are in direct contact with high-temperature steel slag and other media, it must be supplemented with dense particles (<20wt%) to enhance life extension
At the same time, too much silicon oxide in the aluminum-magnesium system can cause the material to produce too much liquid phase at high temperatures, which seriously affects its performance at high temperatures, limits the use temperature of aluminum-magnesium materials, and brings significant "steel" to the molten steel. Oxygenation"

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] An aluminum-magnesium lightweight castable and a preparation method thereof. 60-75wt% aluminum-magnesium porous ceramic particles are used as aggregate, 20-35wt% corundum fine powder, 0.01-0.1wt% silicon oxide fine powder, 3-6wt% magnesium oxide fine powder and 1-4wt% Activated alumina micropowder is used as the base material; 2.5-3wt% superplasticizer of the sum of the aggregate and the base material is premixed with the base material, and then the premixed base material is added to the aggregate, and then the aggregate is added 8-14wt% of water in the sum of base materials is stirred evenly, poured and vibrated and molded, and the molded green body is dried at 110-130° C. for 6-18 hours.

[0025] In this embodiment: the aluminum-magnesium porous ceramic particles are porous corundum ceramics; the corundum fine powder is a mixture of tabular corundum fine powder and white corundum fine powder; A mixture of alumina micropowder; the water reducer is a mixture of sodium ...

Embodiment 2

[0027] An aluminum-magnesium lightweight castable and a preparation method thereof. 65-80wt% aluminum-magnesium porous ceramic particles are used as aggregate, 15-30wt% corundum fine powder, 0.1-0.2wt% silicon oxide fine powder, 2-5wt% magnesium oxide fine powder and 2-5wt% Activated alumina micropowder is used as the base material; add 1.5-2.5wt% superplasticizer of the sum of the aggregate and the base material to pre-mix with the base material, then add the pre-mixed base material to the aggregate, and then add bone 10-16wt% water of the sum of the material and the matrix material is evenly stirred, poured and vibrated for molding, and the molded green body is dried at 120-140° C. for 12-24 hours.

[0028] In this embodiment: the aluminum-magnesium porous ceramic particles are porous corundum ceramics and porous spinel ceramics; the corundum fine powder is a mixture of tabular corundum fine powder and white corundum fine powder; A mixture of aluminum micropowder and activa...

Embodiment 3

[0030] An aluminum-magnesium lightweight castable and a preparation method thereof. 70-85wt% aluminum-magnesium porous ceramic particles are used as aggregate, 10-25wt% corundum fine powder, 0.2-0.3wt% silicon oxide fine powder, 1-4wt% magnesium oxide fine powder and 3-6wt% Activated alumina micropowder is used as the base material; add 1-2wt% water reducing agent of the sum of the aggregate and the base material to pre-mix with the base material, then add the pre-mixed base material to the aggregate, and then add the aggregate The sum of 14-20 wt% water of the base material is evenly stirred, poured and vibrated and molded, and the molded green body is dried at 130-150° C. for 18-36 hours.

[0031] In this embodiment: the aluminum-magnesium porous ceramic particles are porous corundum ceramics, porous corundum-spinel ceramics and porous spinel ceramics; the corundum fine powder is white corundum fine powder; the activated alumina fine powder is activated rho-alumina Mixture ...

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Abstract

The invention relates to an aluminum-magnesium light castable and a preparation method thereof. The technical scheme comprises the following steps: using 60 to 85 wt% of aluminum-magnesium porous ceramic particles as the skeletal material, and using 10 to 35 wt% of corundum fines, 0 to 0.3 wt% of silicon oxide micropowder, 1 to 6 wt% of magnesium oxide micropowder and 2 to 8 wt% of activated aluminum oxide micropowder as the host material; premixing 1 to 3 wt% of water reducer with the host material additionally based on the total weight of the skeletal material and the host material, adding the premixed host material into the skeletal material, and adding 8 to 20 wt% of water additionally based on the total weight of the skeletal material and the host material; and stirring uniformly, pouring, vibration-moulding, and drying the body after the moulding for 6 to 36 hours under the temperature of 110 to 150 DEG C. The product provided by the invention has the characteristics of low silicon content, is cement-free, and has high porosity, small average pore size, high fire resistance, large high temperature strength, low thermal conductivity, good thermal shock stability and strong medium erosion resistance such as the slag and the like. The castable provided by the invention can be used as the energy saving working lining material of the industrial furnace in pyrometallurgy and the like, which can contact with the medium such as the high temperature slag and the like in a long term.

Description

technical field [0001] The invention belongs to the field of castable technology. In particular, it relates to an aluminum-magnesium lightweight castable and a preparation method thereof. Background technique [0002] With the increasing economic development and social progress, energy conservation and emission reduction has become the focus of attention. The development of lightweight insulation materials has been developed rapidly. In terms of lightweight unshaped refractory materials, vermiculite, perlite, ceramsite and fiber castables have been developed. Compared with them, their thermal conductivity is low and they can be used as thermal insulation materials, but their high temperature performance is poor and they are resistant to heat. Slag erosion, especially for alkaline slag, is poor, so it cannot be directly used in industrial furnace linings and other parts in direct contact with slag and other media in high-temperature environments such as metallurgy. [0003...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B35/66
Inventor 顾华志黄奥张美杰杜博
Owner WUHAN UNIV OF SCI & TECH
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