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Method and device for directionally solidifying liquid-solid interface based on alternating magnetic field modulation

A technology of alternating magnetic field and directional solidification, applied in the direction of self-solidification method, chemical instruments and methods, crystal growth, etc., can solve the problem of the decline of casting performance and product qualification rate, the large degree of dendritic trunk geometric center, and the interdendritic shrinkage. and other problems, to achieve the effect of easy operation, maintaining consistent crystal orientation, and reducing defects

Inactive Publication Date: 2012-08-15
SHANGHAI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, in the directional solidification of single crystal superalloys, there are often defects such as miscellaneous crystals, free crystals, freckles, interdendritic shrinkage, and a large degree of dendrite stem deviation from the geometric center of the casting, which greatly reduces the casting performance and product qualification rate, especially in China. The production of single crystal pass rate has been maintained at about 10-50% for a long time

Method used

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  • Method and device for directionally solidifying liquid-solid interface based on alternating magnetic field modulation
  • Method and device for directionally solidifying liquid-solid interface based on alternating magnetic field modulation
  • Method and device for directionally solidifying liquid-solid interface based on alternating magnetic field modulation

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Embodiment 1

[0019] see figure 1 and figure 2 , the method of modulating the liquid-solid interface of directional solidification based on the alternating magnetic field, is characterized in that an alternating magnetic field is added above the liquid-solid interface around the crystallizer, and the induced current and magnetic field in the melt are coupled together by the alternating magnetic field to generate electromagnetic Stirring force, the magnitude, direction and frequency of the electromagnetic stirring force are related to the properties of the melt itself, and the smooth solid-liquid interface of the melt can be obtained by modulating the magnitude, direction and frequency of the electromagnetic field.

Embodiment 2

[0021] This embodiment is basically the same as Embodiment 1, and the special features are as follows: the electromagnetic stirring force is only used to eliminate the temperature difference in the radial direction, and the Joule heating effect is negligible; the magnitude of the electromagnetic stirring force is related to the magnetic field intensity B of the alternating magnetic field 0 Related, the magnetic field strength where u A For Alvin speed ≈ 10 -2 m / s, μ is the magnetic permeability of the melt, and ρ is the density of the melt; the direction of the electromagnetic stirring force is adjusted by changing the distance L between the lower end of the induction coil (4) that generates the alternating magnetic field and the solid-liquid interface of the melt, The range of L is -10 ~ 10mm. The frequency of the electromagnetic stirring force Among them, σ is the electrical conductivity of the sample melt, δ is the skin depth of the solid sample, and the skin effect sh...

Embodiment 3

[0023] This embodiment includes graphite tube main heating body 1, furnace body 2, vacuum system 3, copper induction coil 4, graphite tube auxiliary heating body 5, liquid Ga-In coolant 6, cooling cylinder 7, boron nitride cover 8 , liquid phase sample 10, solid-liquid interface 11, heat insulation layer 12, solid phase sample 13, water cooling system 14, drawing system 15, frequency conversion induction power supply 16; the sample is a superalloy, its length is 150mm, and its diameter is 12mm.

[0024] The graphite tube main heating body 1 and the auxiliary heating body 5 are resistance heaters with a height of 200 mm and 5 mm respectively, the outer diameter of the crucible is 14 mm, the distance between the corundum crucible 9 and the graphite tube main heating body 1 is 2 mm, and the auxiliary heating body 5 is located at The distance between the lower end of the main heating body 1 and the corundum crucible 9 is 1 mm, the copper induction coil 4 is located 5 mm above the ...

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Abstract

The invention relates to a method and device for directionally solidifying a liquid-solid interface based on alternating magnetic field modulation. In the method, an alternating magnetic field is added above the liquid-solid interface at the periphery of a crystallizer, induction current of the alternating magnetic field in a melt is coupled with the magnetic field to generate electromagnetic stirring power, the magnitude, direction and frequency of the electromagnetic stirring power are relevant to the properties of the melt body, and a flat melt liquid-solid interface can be obtained by modulating the magnitude, direction and frequency of the electromagnetic field. In the device, an adjustable copper inductance coil which can generate an alternating magnetic field is sheathed at the periphery of a main heating body in a furnace body, and the inductance coil is connected with a frequency-conversion induction power supply. In the invention, the magnetic field is modulated by adopting the method, an external alternating power supply and an internal adjustable magnetic induction coil are regulated on the structure, the melt flowing can be accurately controlled, the solute and temperature are re-coupled to be homogenized, the planar interface growth of the liquid-solid interface of the solidification material is ensured, the disadvantages are reduced, the crystal orientation is consistent and the efficiency is improved.

Description

technical field [0001] The invention relates to a method and device for modulating a directional solidification liquid-solid interface based on an alternating magnetic field, which is used for controlling crystal growth modes and belongs to the field of material preparation. Background technique [0002] Directional solidification is an important means of material preparation and crystal growth. One of the most important applications in structural materials is to obtain superalloy columnar crystals and single crystals. Single crystal superalloys have become the first choice and development trend for important parts of advanced aviation and gas engines in recent years because of their excellent mechanical properties such as creep resistance, thermal shock resistance, and fatigue resistance. However, in the directional solidification of single crystal superalloys, there are often defects such as miscellaneous crystals, free crystals, freckles, interdendritic shrinkage, and a l...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C30B11/00C30B29/52B22D27/02B22D27/04
Inventor 任维丽樊亚夫任忠鸣钟云波邓康雷作胜
Owner SHANGHAI UNIV