Disinfecting active film as well as preparation method and application thereof
A film and active technology, applied in the field of medical devices, can solve the problems that bacteria and viruses do not have a broad spectrum, affect the comfort and breathability of use, and the targeted efficiency is uncertain, etc., to achieve effective filtration and elimination, High safety and low cost effect
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example 1
[0026] Example 1: Add 64 g of polytetrahydrofuran diol with a relative molecular mass of 2000 and 51.2 g of polyethylene glycol with a relative molecular mass of 80 into a four-necked flask, seal it and pass nitrogen gas at 120° C. for 1.5 hours to remove water. At 65°C, under normal pressure, 25.7 g of isophorone diisocyanate and 20 g of methyl ethyl ketone were added, and the mixture was reacted at 85°C for 4 hours. Then, 40 g of a butanone solution containing 3.48 g of ethylenediamine was added. React for 2 hours. The butanone solvent was removed under reduced pressure at 70°C, and the material was discharged. The crude product was moved to a vacuum drying oven, and dried at 100° C. and a vacuum degree of 0.5 MPa for 24 hours to obtain a polyurethane pressure-sensitive adhesive. Then 10 g of polyurethane pressure-sensitive adhesive and 10 g of 5% ethanol solution of ribavirin are mixed evenly at 80° C. and coated on the non-woven fabric.
Embodiment 2
[0028] Add 40 g of polyoxypropylene diol with a relative molecular mass of 2000 and 100 g of polyethylene glycol with a relative molecular mass of 1000 into a four-necked flask, seal it and ventilate nitrogen at 120° C. for 2 hours to remove water. At 65°C, under normal pressure, 70 g of 1,6-hexamethylene diisocyanate and 70 g of butanone were added, and the mixture was reacted at 85°C for 4 hours. Add ethylenediamine / butanone mixed solution (2.62 g of ethylenediamine, 30 g of butanone), and react for 2 hours. The butanone solvent was removed under reduced pressure at 70°C, and the material was discharged. The crude product was moved to a vacuum drying oven, and dried at 100° C. for 24 hours under a vacuum degree of 0.1 MP to obtain a polyurethane pressure-sensitive adhesive. Then 10 g of polyurethane pressure-sensitive adhesive and 10 g of 1% ethanol solution of zanamivir were mixed uniformly at 80° C., and coated on the polyvinyl chloride film.
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