Composite getter for maintaining medium and low vacuum environment and preparation method thereof
A getter, low vacuum technology, applied in mixed gas absorption, chemical instruments and methods, electrical components, etc., can solve the problems of negative impact of vacuum degree, small effective area, increased cost, etc., to achieve high production efficiency and increased investment. , the effect of improving product quality
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[0044] Preparation of getter metal elemental materials:
[0045] Heat the iron powder with a particle size within the range of 10-200 microns in a hydrogen furnace, and keep it for 120 minutes when the furnace temperature reaches 500°C, or keep it for 90 minutes when the furnace temperature reaches 600°C, or when the furnace temperature reaches 700°C Insulate for 45 minutes, take out the vacuum package after cooling with the furnace, and obtain the iron powder of the scale required by the present invention through reduction treatment, and put the iron powder into a glove box with an argon atmosphere for use.
[0046] Heat the copper powder with a particle size within the range of 10-200 microns in a hydrogen furnace, and keep it for 120 minutes when the furnace temperature reaches 450°C, or keep it for 90 minutes when the furnace temperature reaches 600°C, or when the furnace temperature reaches 700°C Insulate for 60 minutes, take out the vacuum package after cooling, and prom...
Embodiment 1
[0063] The first composite getter of the present invention was prepared. The desiccant powder is selected from the calcium oxide powder prepared by the aforementioned method, and the calcium oxide powder is selected from a particle size of 100-200 microns, because the desiccant powder used in the rotary corer needs coarser particles to increase its flow. properties; the getter metal elemental powder is selected from the iron powder that has been reduced by the aforementioned method, and the iron powder is selected from a particle size of 10-38 microns; the getter alloy powder is selected from the strontium-lithium alloy powder prepared by the aforementioned method, and the strontium-lithium The alloy powder is selected to have a particle size of 50-75 microns.
[0064] In the glove box of the argon environment with the water and oxygen content less than 1ppm, use a tablet press at 25kg / cm 2 The above-mentioned strontium-lithium alloy powder with a weight of 0.5 grams is compr...
Embodiment 2
[0075] Prepare the second composite getter of the present invention. The desiccant powder is selected from the calcium oxide powder prepared by the aforementioned method, and the calcium oxide powder is selected from a particle size of 20-75 microns; The getter alloy powder is 83.18% barium-lithium alloy powder prepared by the aforementioned method, and the getter alloy powder has a particle size of 75-120 microns.
[0076] In a glove box in an argon environment with water and oxygen content less than 1ppm, the composite getter core-coated structure is pressed with a tablet press. Put the above-mentioned calcium oxide powder with a weight of 3 grams into a mold with a diameter of 30 mm in the tablet machine, get 1 gram of the above-mentioned reduced iron powder and add it to the middle position on the calcium oxide powder in the mold, and then add 0.5 grams of the calcium oxide powder. The above-mentioned barium-lithium alloy powder is covered with reduced iron powder, and fi...
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