Preparation method of environment-friendly type emulsion for water-based ink
A water-based ink, environmentally friendly technology, applied in the direction of ink, applications, household appliances, etc., can solve the problems that are difficult to improve, water-based ink leveling, alcohol dilution and salt resistance performance are slightly poor, to achieve enhanced bonding strength, High bond strength, good product leveling effect
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Embodiment 1
[0021] (1). Preparation of water-soluble resin
[0022] Add 133g of water, 0.11g of AES 48E and 0.12g of baking soda into the reaction kettle, start stirring, raise the temperature to 78°C, add 0.90g of ammonium persulfate solution diluted with 5.0g of water, then dropwise add 29.0g of ethyl acrylate, formaldehyde Acrylic acid 7.4g, tert-dodecyl mercaptan 2.2g mixed monomer, dripping within 45min, the stirring speed is controlled at 100-150 rpm, and the temperature is controlled at 76-78°C. After the dropwise addition, add ammonia water to adjust the pH to 8.0-8.5, and set aside.
[0023] (2). Preparation of environment-friendly emulsion for water-based ink
[0024] Add AEO355.0g to the above-mentioned water-soluble resin, stir until dissolved, add 10% polymerized monomer (126.0g styrene, 16.0g butyl acrylate) at 78°C, add initial initiator (13.0g water, persulfuric acid ammonium 1.45g), and then drop the remaining monomers, and finish dropping within 2-3 hours. The stirring...
Embodiment 2
[0027] The polymerized monomers were 67g of styrene, 50g of butyl acrylate, and 130g of isooctyl, and the other formulations and processes were the same as in Example 1.
[0028] The water-based ink prepared with the emulsion is soft, low temperature resistant and particularly good in adhesion.
Embodiment 3
[0030] The polymerized monomers were 134g of styrene and 8g of butyl acrylate, and the other formulations and processes were the same as in Example 1.
[0031] Mixing the emulsion with the emulsion prepared in Example 2 to prepare water-based ink can greatly reduce the cost and improve the hardness and gloss.
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