Method for purifying gibberellin GA3 and preparing water-soluble pulvis of gibberellin GA3
A technology of water-soluble powder and gibberellin, applied in botany equipment and methods, biocides, animal repellants, etc., can solve the problems of increasing product size, reducing dissolution rate, increasing production cost, etc., and achieves easy precipitation, Easy to use, fine and uniform purity effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0019] Add water 2 Kg, tetrahydrofuran 2 Kg and ethyl acetate 4 Kg successively in 10 L reactor, stir for ten minutes, make each component mix evenly, drop into crystalline powder crude product 500 g, crude product purity (GA 3 content) to 78%, heated up to 35~40 ℃ to dissolve completely, added 0.5 g of activated carbon, kept stirring for 30 minutes, and filtered with suction. The jacket temperature is controlled at 65°C, the cooling rate is 8°C / hour, the stirring rate is 200 rpm, concentrated to 5% of the mother liquor volume, and gibberellin GA is separated out 3 Crystallized, separated and dried to obtain gibberellin GA 3 The original powder is 382 g, the powder purity is 99%, and the rate of crystal size passing through a 300-mesh sieve reaches 98%.
Embodiment 2
[0021] Add the purified gibberellin GA in turn to the mixer 3 30 g of raw powder, 15 g of sodium silicate, 40 g of sodium dihydrogen phosphate, 8 g of domiphene, 5 g of sugar and 2 g of vitamin C, stirred for 30 min to mix all components evenly, and dried the obtained mixture at 50 °C , bagged, to get gibberellin GA 3 Water-soluble powder. After testing, the suspension rate is above 97%, and the wetting time is less than 30 s, meeting the quality standards of water-soluble powder.
Embodiment 3
[0023] Add the purified gibberellin GA in turn to the mixer 3 20 g of raw powder, 20 g of sodium silicate, 45 g of sodium dihydrogen phosphate, 8 g of domiphene, 5 g of sugar and 2 g of vitamin C, stirred for 30 min to mix all components evenly, and dried the obtained mixture at 50 °C , bagged, to get gibberellin GA 3 Water-soluble powder. After testing, the suspension rate is above 98%, and the wetting time is less than 30 s, meeting the quality standard of water-soluble powder.
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com