Method for preparing binary copolymer retarder for oil and gas well cementing
A binary copolymer, well cementing technology, applied in chemical instruments and methods, drilling compositions and other directions, can solve the problems of complex raw materials and the effect of cement retarder retarding effect, etc., and achieve simple and good compatibility of raw materials The effect of sex, excellent technical effect
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[0037] Example 1
[0038] The invention discloses a preparation method of a binary copolymer retarder for cementing oil and gas wells. The steps include:
[0039] (1) Dissolve 2-acrylamide-2-methylpropanesulfonic acid and itaconic acid in 200% deionized water of the total monomer mass according to the mass ratio of 73~75:25~27;
[0040] (2) Adjust the pH value of the solution in step (1) to 5~6 with a 50% mass volume concentration NaOH solution;
[0041] (3) place the solution obtained in step (2) in a three-necked flask, carry out a constant temperature water bath, and heat up to 60~65°C;
[0042] (4) dropwise adding an initiator accounting for 1.0% to 2.0% of the total monomer mass to the solution obtained in step (3), and the reaction time is continued for 4 to 6 hours to obtain the final product.
[0043] The retarder prepared by the above steps, compared with the existing similar technology, the present invention has the following technical advantages:
[0044] The met...
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[0048] Example 2
[0049] The preparation method of the binary polymer retarder of the present invention is as follows:
[0050] According to the mass ratio of 75:25, 2-acrylamide-2-methylpropanesulfonic acid and itaconic acid were respectively weighed and dissolved in 200% deionized water of the total monomer mass; pH was adjusted with 50% mass volume concentration NaOH solution To 6; the solution was placed in a three-necked flask with a thermometer and a stirrer, the temperature in a constant temperature water bath was heated to 60 ° C, and an initiator potassium persulfate, which accounted for 2.0% of the total monomer mass, was added dropwise to the solution within 30 min, and the reaction time was 4 hours. The final product is obtained, a binary copolymer retarder.
[0051] The effect of the present invention is:
[0052] The retarder can effectively prolong the thickening time of cement slurry in the temperature range of 50~180℃. Taking Jiajiang Grade G cement as an ex...
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