Lutein ester microcapsule powder and preparation method thereof

A technology of lutein ester and microcapsule powder is applied in the field of preparation of cold water dispersible lutein ester microcapsule powder, can solve problems such as limiting the scope of application fields, and achieves green environmental protection technology, good stability and uniform color long lasting effect

Active Publication Date: 2012-03-28
INNOBIO CORP LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, due to the oil solubility of lutein esters limits its application range, the development of nano-scale cold water dispersible lutein ester microcapsule powder can not only directly apply lutein esters to water system food coloring, but also nano-scale Particle size can be better absorbed by the body

Method used

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  • Lutein ester microcapsule powder and preparation method thereof
  • Lutein ester microcapsule powder and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1~4

[0027] Prepare lutein ester microcapsule powder, first according to Table 1 ingredients (unit: gram):

[0028] Table 1

[0029] raw material name

Example 1

Example 2

Example 3

Example 4

Lutein Ester Crystals (Purity 68%)

1.5g

7.5g

15g

30g

dl-α-tocopherol: mixed natural VE (weight ratio) = 1:1

0.15g

0.75g

1.5g

3g

Glyceryl monostearate

0.15g

0.75g

1.5g

3g

Glyceryl Caprylate

1.5g

3.5g

7g

10g

OSA-modified gum arabic

10g

18g

23g

30g

Sucrose palmitate: modified soybean lecithin (weight ratio) = 1: 2.5

0.15g

3.75g

7g

10g

Sodium ascorbate: tea polyphenols (weight ratio) = 2:1

0.15g

0.75g

1.5g

3g

White sugar

86.4g

72.5g

58.5g

41g

water

100g

200g

450g

900g

[0030] ① Weigh lutein...

Embodiment 5~8

[0038] Prepare lutein ester microcapsule powder, first according to Table 3 ingredients (unit: gram):

[0039] table 3

[0040] raw material name

Example 5

Example 6

Example 7

Example 8

Lutein Ester Crystals (Purity 68%)

1.5g

7.5g

15g

30g

dl-alpha-tocopherol

0.075g

0.52g

0.75g

1.2g

glyceryl monooleate

0.12g

0.68g

0.60g

0.60g

Glyceryl Caprylate

0.22g

7.5g

0.75g

24g

OSA-modified gum arabic

37.5g

22.5g

15g

18g

Modified Soy Lecithin

0.3g

2.6g

6.5g

14.4g

sodium ascorbate

0.12g

3.0g

0.75g

7.5g

glucose

60.165g

55.7g

60.65g

4.3g

water

150g

300g

450g

500g

[0041]① Weigh lutein ester crystals, dl-α-tocopherol, glyceryl monooleate and glyceryl caprylate according to the above tabl...

Embodiment 9~12

[0049] Prepare lutein ester microcapsule powder, first according to Table 5 ingredients (unit: gram):

[0050] table 5

[0051] raw material name

Example 9

Example 10

Example 11

Example 12

Lutein Ester Crystals (Purity 68%)

1.5g

7.5g

15g

30g

Mix natural VE

0.11g

0.6g

0.9g

2.8g

glyceryl monolaurate

0.10g

0.33g

0.70g

2.3g

sunflower oil

3g

15g

9g

10g

OSA-modified starch

30g

24g

45g

30g

Sucrose Stearate

0.65g

2.55g

3.5g

3.3g

Tea polyphenols

0.25g

1.5g

1.2g

3.2g

Isomaltooligosaccharide

64.39g

48.52g

24.7g

18.4g

water

200g

250g

500g

600g

[0052] ① Weigh lutein ester crystals, dl-α-tocopherol, glyceryl monooleate and glyceryl caprylate according to the above table 5, mix thoro...

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Abstract

The invention discloses lutein ester microcapsule powder and a preparation method thereof. The preparation method comprises the following steps of: preparing an oil phase solution and a water phase solution respectively, and mixing and emulsifying the oil phase solution and the water phase solution; and non-water raw materials comprise the following components in part by weight: 1 part of lutein ester crystal, 0.05 to 0.1 part of oil phase antioxidant, 0.02 to 0.1 part of oil phase emulsifying agent, 0.05 to 1 part of plant oil, 0.5 to 25 parts of wall material, 0.1 to 0.5 part of water phaseemulsifying agent, 0.05 to 1 part of water phase antioxidant, and the balance of filler. In the preparation method for the lutein ester microcapsule powder, the oil-soluble lutein ester is fully dispersed in cold water in the form of sub nanometer particles, and the product can be self-emulsified in water, and is good in instant capacity and self-emulsification capacity, and high in stability, and has uniform and durable color; and the phenomena of oil floating, precipitation, adhesion to a bottle wall and the like are avoided during application. Organic solvents are not introduced in the powder, so solvent residues are avoided in the product. The production process is environment-friendly, simple and practicable, expensive equipment is not needed, and the microcapsule powder can be industrially produced easily and conveniently.

Description

technical field [0001] The invention relates to a preparation method of cold water dispersible lutein ester microcapsule powder. Background technique [0002] Lutein esters are carotenoid fatty acid esters that exist in the form of fatty acids combined with lutein. It is widely found in plants such as pumpkins, cabbage, spinach, and marigold flowers. Among them, the content is the most abundant in marigold flowers. Research has shown that intake of lutein esters increases lutein levels in blood and in the macula of the retina, thereby preventing age-related retinoid degeneration (Snodderly D.M.Am.J.Clin.Nutr.62(suppl.): 144805- 618, 1995) and cataracts (Lisa C.T, et al. Am. J. Clin Nutr. 90:509-15, 1999). And it can effectively inhibit tumor growth and prevent the occurrence of atherosclerosis (James D, et al. Circulation. 103: 2922, 2001). [0003] In actual production, the stability of lutein ester to light, heat and acid is stronger than that of lutein. It is of great...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A23L1/29A23L33/00
Inventor 吴文忠黄媛陈剑彬陈碧聪吕忠武刘强
Owner INNOBIO CORP LTD
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