Photocatalysis compound filling material for micro pollution raw material pretreatment and preparation method thereof
A composite filler and pretreatment technology, which is applied in the directions of light water/sewage treatment, oxidized water/sewage treatment, etc., can solve the problems of unsatisfactory photocatalytic efficiency, difficult industrialization, and insufficient firmness, and achieves improved photocatalytic activity. , The effect of strong fluidity and easy operation
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[0025] Example 1: Mix 20 mg of titanate coupling agent and 10 mL of ethanol, heat to 80°C, stir uniformly, and after reacting for 3 hours, add 1% TiO by mass 2 Powder, and fully stir until the ethanol boils and volatilizes to a very small amount of solvent (about 1-2ml), and then repeatedly add the same mass ratio of ethanol. Follow the above method and repeat 2 times. Put the obtained thick colloid in an oven, adjust the temperature to 80° C., dry for 12 hours, and crush and grind the obtained solid for use.
[0026] The polypropylene raw material and pretreated TiO 2 Blended on twin screw extruder, TiO 2 The mass fraction is 8%. The material is fed into the screw groove of the screw from the feeding port, so that the polypropylene raw material is gradually melted into a melt in the screw groove. When the temperature is 180°C and the pressure is 78kPa, it is outputted and extruded by the screw. Formed into oblique rotation. The prepared composite filler has a diameter of 15-25m...
Example Embodiment
[0027] Example 2: Mix 25 mg of titanate coupling agent and 15 mL of ethanol, heat to 85°C, stir evenly, and after 4.5 hours of reaction, add 1.5% TiO by mass 2 Powder, and fully stir until the ethanol boils and volatilizes to a very small amount of solvent (about 1-2ml), and then repeatedly add the same mass ratio of ethanol. Follow the above method and repeat 3 times. Put the obtained thick colloid in an oven, adjust the temperature to 85°C, dry for 18 hours, and crush and grind the obtained solid for use.
[0028] The polypropylene raw material and pretreated TiO 2 Blended on twin screw extruder, TiO 2 The mass fraction is 9%. The material is fed into the screw groove of the screw from the feeding port, so that the polypropylene raw material is gradually melted into a melt in the screw groove. When the temperature is 190℃ and the pressure is 94kPa, the material is outputted and extruded by the screw. Formed into oblique rotation. The prepared composite filler has a diameter of...
Example Embodiment
[0029] Example 3: Mix 30 mg of titanate coupling agent and 20 mL of ethanol, heat to 90°C, stir uniformly, and after reacting for 6 hours, add 2% TiO by mass 2 Powder, and fully stir until the ethanol boils and volatilizes to a very small amount of solvent (about 1-2ml), and then repeatedly add the same mass ratio of ethanol. Follow the above method and repeat 4 times. Put the obtained thick colloid in an oven, adjust the temperature to 95°C, dry for 24 hours, and crush and grind the obtained solid for use.
[0030] The polypropylene raw material and pretreated TiO 2 Blended on twin screw extruder, TiO 2 The mass fraction is 10%. The material is fed into the screw groove from the feeding port, so that the polypropylene raw material is gradually melted into a melt in the screw groove. When the temperature is 200℃ and the pressure is 110kPa, it is outputted and extruded by the screw. Formed into oblique rotation. The prepared composite filler has a diameter of 15-25mm, a height of...
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