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Method for quickly preparing special gelatin for candies from raw bone meal

A raw bone meal and candy technology, applied in the field of gelatin preparation, can solve the problems of gelatin viscosity and gel strength mismatch

Active Publication Date: 2012-05-02
NINGXIA XINHAOYUAN BIOLOGICAL POLYTRON TECH INC
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Aiming at the fact that there is no special gelatin specially used for the candy industry in the current gelatin production industry and other gelatins that cannot fully meet the requirements of the candy industry, that is, the problem that the viscosity of the gelatin does not match the freezing strength, the present invention proposes a kind of raw bone powder for rapid preparation of candy. The method for gelatin, the technical solution adopted by the present invention is: a method for quickly preparing gelatin for candy from raw bone meal, which is characterized in that it consists of the following steps: grinding animal bone powderpickling to remove impurities → washing → extracting glue → Neutralization→coarse filtration→fine filtration→concentration and drying packaging; among them: the technological conditions of the animal bone grinding process are: grinding animal bones into 40-160 mesh raw bone powder; the technological conditions of the pickling and impurity removal process are: grinding The raw bone meal is soaked in the acid solution at a temperature of 15°C-25°C for 6-12 hours to remove impurities such as minerals in the raw bone meal. The pH value of the acid solution is 1-2.5, and the mass volume of the raw bone meal and acid solution The ratio is 1g:2-6ml; the process conditions of the washing process are: the raw bone meal soaked in acid solution is washed with water until the pH of the washing water is 4-6; the process conditions of the glue extraction process are: the washed bone meal Raw bone meal extracts the glue solution after 5 to 18 hours under lye at a temperature of 40°C to 70°C, the pH of the lye is 8 to 14, and the mass volume ratio of raw bone meal to lye is 1g:4 to 10ml; The process conditions of the neutralization process are: adjust the pH value of the extracted glue to 5.5-6.5 with acid; the process conditions of the coarse filtration process are: use a filter to filter the neutralized extract Filtration at low temperature to separate the gelatin liquid from the solid residue; the process conditions of the fine filtration process are: finely filter the gelatin liquid after the coarse filtration at a temperature of 40°C to 60°C; the process conditions of the concentrated drying and packaging process are: The fine filtrate is concentrated and dried by conventional methods

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0004] Example 1: A method for rapidly preparing candy-specific gelatin from raw bone meal. 1000 grams of animal bone is ground into 40-mesh bone meal, soaked in 2000 ml of nitric acid solution with a temperature of 25 ° C and a pH value of 1 for 12 hours, and the Impurities such as minerals in the raw bone meal, the raw bone meal soaked in acid solution is washed with water until the pH value of the washing water is 6, and the raw bone meal after washing is washed at a temperature of 70°C, a pH value of 14, and 4000 ml of sodium carbonate alkali After 5 hours of extracting the glue under the liquid, neutralize the extracted glue with acid, adjust the pH value to 5.5, and carry out secondary coarse filtration of the neutralized solution at a temperature of 60°C with a vacuum filter and a plate-and-frame filter. The filtrate is then carried out secondary fine filtration with membrane filtration and ion exchange filtration at a temperature of 60° C., and the fine filtrate is conc...

Embodiment 2

[0007] Example 2: A method for rapidly preparing candy-specific gelatin from raw bone meal. Grind 1000 grams of animal bone into 160-mesh bone meal, soak it in 6000 ml of phosphoric acid solution with a temperature of 15°C and a pH value of 2.5 for 6 hours, remove Impurities such as minerals in the raw bone meal, the raw bone meal soaked in acid solution is washed with water until the pH value of the washing water is 4, and the raw bone meal after washing is washed at a temperature of 40°C, a pH value of 8, and 10,000 ml of sodium bicarbonate After 18 hours of extracting the glue under alkali solution, neutralize the extracted glue with acid, adjust the pH value to 6.5, and carry out secondary coarse filtration of the neutralized solution at a temperature of 40°C with a vacuum filter and a plate-and-frame filter , then the filtrate is carried out secondary fine filtration with membrane filtration and ion-exchange filtration at a temperature of 40°C, and the fine filtrate is con...

Embodiment 3

[0010] Example 3: A method for rapidly preparing candy-specific gelatin from raw bone meal. Grind 1000 grams of animal bone into 120-mesh bone meal, soak it in a hydrochloric acid solution with a temperature of 20 ° C, a pH value of 2, and 4000 ml for 8 hours. Impurities such as minerals in the raw bone meal, the raw bone meal soaked in acid solution is washed with water until the pH value of the washing water is 5, and the raw bone meal after washing is washed with potassium hydroxide at a temperature of 50°C, a pH value of 10, and 8000 ml of potassium hydroxide. After 15 hours of extracting the glue with the compound lye of calcium hydroxide, neutralize the extracted glue with acid, adjust the pH value to 6, and filter the neutralization solution with a vacuum filter and a plate frame at a temperature of 45°C The machine carries out secondary coarse filtration, and then the filtrate is carried out secondary fine filtration with membrane filtration and ion exchange filtration ...

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PUM

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Abstract

The invention belongs to the field of gelatin preparation, and particularly relates to a method for quickly preparing special gelatin for candies from raw bone meal. The method comprises the following process steps of: meal milling, impurity removal through pickling, water washing, gelatin solution extraction, neutralization, rough filtration, fine filtration, and packaging after concentration and drying. According to the method, animal bones are milled into bone meal to increase the specific surface area of the bone meal and increase the reaction speed of the bone meal; and compared with thetraditional gelatin production, the method disclosed by the invention has the advantages that: the production cycle is shortened by more than 60 days, and pollution and consumption are reduced. The gelatin prepared by using the method has the advantages of high freezing intensity, moderate viscosity, good transparency and low cost; and the viscosity of the gelatin is matched with the freezing intensity of the gelatin, so that the gelatin is suitable for the field of producing foods such as candies and the like.

Description

1. Technical field: [0001] The invention belongs to the field of gelatin preparation, in particular to a method for rapidly preparing gelatin for candy from raw bone meal. 2. Background technology [0002] At present, the production of bone gelatin in my country all adopts the traditional alkaline process, and its process route is: animal bone → bone grains → picklingwater washing → liming → water washingneutralization → water washing → gel extractionfiltration → concentration → drying → pulverization. Although the traditional gelatin has a history of hundreds of years and the technology is relatively mature, the production cycle is long, as long as 60 to 90 days, and the consumption of various materials is high, especially the waste of water resources. The traditional liming process uses milk of lime. A large amount of ash and waste water are produced every day, which belongs to high energy consumption and high pollution industries, and when its gelatin products ar...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09H3/00C09H3/02A23G3/36
Inventor 逯益民牟忠臣
Owner NINGXIA XINHAOYUAN BIOLOGICAL POLYTRON TECH INC