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Preparation method of aluminum pigment with high voltage breakdown resistance

A technology of voltage resistance and aluminum pigments, which is applied in the direction of fibrous filler, dyeing polymer organic compound treatment, dyeing physical treatment, etc., can solve the problem of insufficient voltage resistance performance, instantaneous voltage rise on the surface of the casing, impossible voltage resistance performance, etc. Problems, to achieve high withstand voltage performance, convenient construction, not easy to damage the effect

Inactive Publication Date: 2012-07-25
HEFEI SUNRISE PIGMENTS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] However, the use of traditional non-encapsulated aluminum pigments in recent years has also exposed some problems that are difficult to overcome.
For example, the voltage resistance performance of the coating on the outer surface of home appliances formulated with it is significantly insufficient. As the structure of home appliances is developing towards light weight, compactness, and maximum space utilization, the instantaneous voltage on the surface of the casing during the switching process of home appliances is also Due to the limitations of the traditional non-encapsulated aluminum pigment production process, it is impossible to have a higher withstand voltage performance

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] This embodiment includes the following steps:

[0022] Step 1: Take 60 kg of raw material spherical aluminum powder, 1.2 tons of grinding medium steel balls with a diameter of 0.8 mm, 120 kg of D80 solvent oil, 0.36 kg of oleic acid, and 0.2 kg of vinyl triethoxysilane and put them into the ball mill;

[0023] Step 2: Seal the ball mill, ball mill at a speed of 60r / min for 10 hours, adjust the speed of the ball mill to 20r / min, ball mill for 2 hours, and discharge with environmentally friendly solvent oil;

[0024] Step 3: Input the material into the vibrating screen through the pipeline for screening and classification, remove the residue from the screen, and enter the plate and frame filter press for pressure filtration to obtain a filter cake with a solid content of 75%;

[0025] Step 4. Add the obtained filter cake with a solid content of 75% and 160 kilograms of propylene glycol methyl ether acetate solvent into the reactor together, seal the reactor, and raise the temperat...

Embodiment 2

[0027] This embodiment includes the following steps:

[0028] Step 1: Take 50 kg of raw material spherical aluminum powder, 1.2 tons of grinding media steel balls with a diameter of 1.0 mm, 80 kg of D70 solvent oil, 0.20 kg of oleic acid, and 0.1 kg of vinyl tris (2-methoxyethoxy) silane Put into the ball mill;

[0029] Step 2: Seal the ball mill, ball mill at a speed of 60r / min for 10 hours, adjust the speed of the ball mill to 20r / min, ball mill for 2 hours, and discharge with environmentally friendly solvent oil;

[0030] Step 3: Input the material into the vibrating screen through the pipeline for screening and classification, remove the residue from the screen, and enter the plate and frame filter press for pressure filtration to obtain a filter cake with a solid content of 75%;

[0031] Step 4. Add the obtained filter cake with a solid content of 75% and 120 kg of butyl acetate solvent into the reaction vessel together, seal the reaction vessel, and raise the temperature of the ...

Embodiment 3

[0033] This embodiment includes the following steps:

[0034] Step 1. Take 40 kilograms of raw material spherical aluminum powder, 1.2 tons of grinding media steel balls with a diameter of 1.2 mm, 100 kilograms of D60 solvent oil, 0.30 kilograms of oleic acid, and 0.15 kilograms of γ-methacryloxypropyltrimethoxysilane Put into the ball mill;

[0035] Step 2: Seal the ball mill, ball mill at a speed of 60r / min for 10 hours, adjust the speed of the ball mill to 20r / min, ball mill for 2 hours, and discharge with environmentally friendly solvent oil;

[0036] Step 3: Input the material into the vibrating screen through the pipeline for screening and classification, remove the residue from the screen, and enter the plate and frame filter press for pressure filtration to obtain a filter cake with a solid content of 75%;

[0037] Step 4. Add the obtained filter cake with a solid content of 75% and 140 kg of ethanol solvent into the reaction kettle together, seal the reaction kettle, and unde...

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PUM

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Abstract

The invention discloses a preparation method of an aluminum pigment with high voltage breakdown resistance. The method comprises the steps of putting raw materials including spherical aluminum powder, a grinding medium, an environment-friendly solvent oil, oleic acid or erucic acid, and a silicane coupling agent into a ball mill; sealing the ball mill, performing ball milling, and discharging the materials with the environment-friendly solvent oil; conveying the materials through a pipeline into a vibration screen to be screened, removing screen tailings, and putting the materials into a frame filter press to conduct filter pressing, so as to obtain filter cakes with a solid content of 75%; feeding the filter cakes and an alcohol, ether or ester solvent into a reaction kettle, sealing the reaction kettle, increasing temperature under the protection of inert gases, then simultaneously dripping acrylic acid or acrylate monomer and an azo type initiator, continuously increasing the temperature of the reaction kettle, keeping the temperature, discharging materials, and performing filter pressing, so as to obtain the finished product. The aluminum pigment has the characteristic of high voltage breakdown resistance, the construction is convenient, the environment-friendly solvent oil is adopted for ball milling, and detection of all hazardous substances meets standards established by European Union.

Description

Technical field [0001] The invention relates to a method for preparing a coating for the outer surface of a household appliance, in particular to a method for preparing an aluminum pigment with high voltage resistance. Background technique [0002] With the rapid development of my country’s economy and the rapid development of the domestic home appliance industry, home appliance manufacturing technology and home appliance outer surface coating technology and level continue to rise. As the main silver-white metallic pigment used in the home appliance coating industry, flake aluminum pigments have nearly a market demand. The rapid development of aluminum pigment technology has been developing in the direction of high withstand voltage performance, high coverage rate, good flashing effect and special performance. [0003] However, the use of traditional uncoated aluminum pigments in recent years has also exposed some problems that are difficult to overcome by themselves. For example, ...

Claims

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Application Information

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IPC IPC(8): C09C1/64C09C3/04C09C3/12C09C3/10
Inventor 董前年朱双单
Owner HEFEI SUNRISE PIGMENTS
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