Novel high-consumption resistant multi-element rare earth tungsten electrode and preparation method thereof
A new technology of rare earth tungsten, which is applied in the field of tungsten electrode materials and its preparation, can solve the problems of difficult processing of high-content rare earth tungsten materials and low yield, and achieve the effects of shortening sintering time, improving product yield, and simplifying equipment and technology
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[0018] The present invention will be further described below in conjunction with the technical scheme of the present invention and the traditional process method.
[0019] In a new type of high-durability multi-component rare earth tungsten electrode, the weight ratio of rare earth is Re 2 o 3 : La 2 o 3 : CEO 2 : Y 2 o 3 = 1:2:2:6, the other is W, and the composite rare earth tungsten electrode with a total content of 2.2% is studied through the SPS preparation process, and compared with the traditional "pressing + vertical melting sintering" process, the specific content is as follows:
[0020] Such as figure 1 , described in the process flow chart of the present invention: the invention includes the following steps: 1. Doping, 2. Reduction, 3SPS sintering, 4 swaging, 5 drawing, 6 polishing, and inspection.
[0021] Wherein, in the doping step, a liquid-solid doping method is adopted. Make a solution of rare earth nitrate and deionized water, put a certain weight of ...
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