Integrated circuit (IC) card packaging special hot melting adhesive tape and preparation method thereof
A technology of hot-melt adhesive film and polyamide hot-melt adhesive, which is applied in the direction of adhesive, adhesive type, film/sheet adhesive, etc., which can solve the problem of limited bonding ability, separation of chip module and card substrate, etc. Problems, to achieve fast melting, meet the requirements of production efficiency and bonding effect, reasonable design effect
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[0020] A preparation method of a special hot-melt adhesive film for IC card packaging, comprising the following steps:
[0021] ⑴Preparation of modified polyamide hot melt adhesive solution: add dibasic acid and dibasic amine into the reaction vessel, react for 1 to 2 hours under an inert atmosphere, then drop to normal pressure, add small molecule dibasic alcohol to react 3 ~ 8 hours, then remove excess small molecular diols by distillation under reduced pressure to obtain amide diols; then add the gained amide diols and two functional group isocyanates, catalysts and solvents to another reaction vessel, in an inert The modified polyamide hot-melt adhesive solution is obtained after reacting at a temperature of 70-90°C for 3-5 hours under the atmosphere;
[0022] (2) Preparation of thermally conductive filler dispersion: Add dispersion aid, solvent and thermally conductive filler into a stirred container, and stir for more than 2 hours to obtain thermally conductive filler di...
Embodiment 1
[0026] (1) Preparation of modified polyamide hot-melt adhesive solution: under nitrogen atmosphere, add 71g of sebacic acid, 78g of dimer fatty acid, 58g of hexamethylenediamine, 86g of decanediamine into a pressure vessel equipped with a stirrer, control The pressure inside the reactor is 10×10 5 Pa, the temperature is 200 ° C, after 1.5 hours of reaction, it is reduced to normal pressure, and then 76g of 1,3-propanediol is added, and the pressure is controlled to be 10×10 5 Pa, the temperature is 200°C, after 4 hours of reaction, reduce to normal pressure and remove unreacted small molecule diols by vacuum distillation to obtain amides diols; under nitrogen environment, 90.8g amides obtained above Dihydric alcohol, 26.7g isophorone diisocyanate, 0.5g dibutyltin dilaurate and 120g butanone are added in the reaction vessel, and the temperature is controlled at 85°C under an inert atmosphere for 3 hours and then cooled to room temperature to obtain the modified Polyamide hot m...
Embodiment 2
[0030] (1) Preparation of modified polyamide hot melt adhesive solution: under nitrogen atmosphere, add 71g glutaric acid, 78g adipic acid, 70g pimelic acid, 58g hexamethylenediamine, 86g Decanediamine, control the pressure in the reactor to 10×10 5 Pa, the temperature is 200 ° C, after 1.5 hours of reaction, it is reduced to normal pressure, and then 76g of 1,3-propanediol is added, and the pressure is controlled to be 10×10 5 Pa, the temperature is 200°C, after 4 hours of reaction, reduce to normal pressure and remove unreacted small molecule diols by vacuum distillation to obtain amides diols; under nitrogen environment, 90.8g amides obtained above Dihydric alcohol, 26.7g isophorone diisocyanate, 0.5g dibutyltin dilaurate and 120g butanone are added in the reaction vessel, and the temperature is controlled at 85°C under an inert atmosphere for 3 hours and then cooled to room temperature to obtain the modified Polyamide hot melt adhesive solution.
[0031] (2) Preparation ...
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