Low-permeability reservoir water-lock releasing agent and preparation method thereof
A water-releasing agent and low-permeability technology, applied in chemical instruments and methods, drilling compositions, etc., can solve the problem of unsatisfactory water-locking damage effect, limited application range, and difficulty in taking into account low-permeability reservoir geology and reservoir conditions. And construction technology and other issues, to achieve the effect of removing water lock damage, wide application range, and improving water solubility
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Embodiment 1
[0018] This embodiment discloses a low-permeability oil reservoir dewatering and locking agent and its preparation method. This low-permeability oil reservoir dewatering and locking agent is composed of 50 g ethylene glycol butyl ether, 90 g N·Nˊ-dodecyl-ethylene glycol Sodium aminodipropionate, 70g ethylene glycol triethylsilyl ether, 160g distilled water. The specific preparation method is:
[0019] In a four-necked 500ml flask with a reflux condenser, a thermometer, and a dropping funnel, add 160g of distilled water, put a stirring magnet, put the flask into a magnetic stirrer with an electric heating jacket, turn on the magnetic stirrer, turn on the heating switch, and the temperature Control at 30-40°C, turn on the cooling water of the reflux condenser; add 50 g of ethylene glycol butyl ether, then add 90 g of N·Nˊ-dodecyl-ethylenediamine dipropionate, and react for 1 hour. Add 70g of ethylene glycol triethylsilyl ether, control the temperature at 70-80°C, and react for ...
Embodiment 2
[0021] This embodiment discloses a low-permeability oil reservoir dewatering and locking agent and a preparation method thereof. By mass, this low-permeability oil reservoir dewatering and locking agent is prepared by adding 50 g of polyethylene glycol methyl ether, 115g N.N'-dodecyl- Sodium ethylenediaminodiacetate, 56g ethylene glycol trimethylsilyl ether, 140g distilled water. The specific preparation method is:
[0022] In a four-necked 500ml flask with a reflux condenser, a thermometer, and a dropping funnel, add 140g of distilled water, put a stirring magnet, put the flask into a magnetic stirrer with an electric heating jacket, turn on the magnetic stirrer, turn on the heating switch, and the temperature Control at 30-40°C, turn on the cooling water of the reflux condenser; add 50 g of polyethylene glycol methyl ether, and then add 115 g of N·Nˊ-dodecyl-ethylenediaminodiacetate, and react for 1 hour. Add 56g of ethylene glycol trimethylsilyl ether, control the temperat...
Embodiment 3
[0024] This embodiment discloses a low-permeability oil reservoir dewatering and locking agent and a preparation method thereof. By mass, this low-permeability oil reservoir dewatering and locking agent consists of 35 g diethylene glycol ether, 80 g N.N'-dodecyl-ethylene glycol Sodium aminodipropionate, 75g polyethylene glycol trimethylsilyl ether, 150g distilled water. The specific preparation method is:
[0025] In a four-necked 500ml flask with a reflux condenser, a thermometer, and a dropping funnel, add 150g of distilled water, put a stirring magnet, put the flask into a magnetic stirrer with an electric heating jacket, turn on the magnetic stirrer, turn on the heating switch, and the temperature Control at 30-40°C, turn on the cooling water of the reflux condenser; add 35 g of diethylene glycol ether, then add 80 g of N·Nˊ-dodecyl-ethylenediamine dipropionate, and react for 1 hour. Add 75g of polyethylene glycol trimethylsilyl ether, control the temperature at 65-75°C, ...
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