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89results about How to "Low cloud point" patented technology

Low-permeability reservoir water-lock releasing agent and preparation method thereof

The invention discloses an oil field chemical agent used in petroleum gas oil-pumping operation construction, and particularly relates to a low-permeability reservoir water-lock releasing agent used in working fluid and a preparation method thereof. The low-permeability reservoir water-lock releasing agent consists of the following components in percentage by weight: 1 to 15 percent of glycol ether, 15 to 45 percent of didodecyl dicarboxylic sodium, 15 to 30 percent of ethylene glycol silicon ether and 30 to 60 percent of water. The preparation method comprises the following steps of: adding 30 to 60 percent of water into an enamel reaction kettle, starting a stirrer, and heating to raise the temperature to be between 30 and 40 DEG C; adding 1 to 15 percent of glycol ether and 15 to 45 percent of didodecyl dicarboxylic sodium into the reaction kettle, controlling the temperature and stirring for 1 hour; and adding 15 to 30 percent of ethylene glycol silicon ether into the reaction kettle, controlling the temperature to be between 40 and 80 DEG C, and reacting for 1 to 2 hours to obtain the water-lock releasing agent. The water-lock releasing agent is strong in surface activity and low in use level, can well maintain the permeability of a low-permeability reservoir and release water-lock damages, and is used in the working fluid such as fracturing fluid, perforating fluid, well control fluid and the like.
Owner:唐山冀油瑞丰化工有限公司 +1

Preparation method of condensation point reducer with dual functions of reducing condensation point and turbidity point

The invention provides a preparation method of a condensation point reducer with dual functions of reducing condensation point and turbidity point, which comprises the following steps: (1) mixing C8-C18 straight-chain fatty alcohols and methacrylic acid in a mol ratio of (1.02-1.2):1, adding diluent oil as a solvent, adding a polymerization inhibitor hydroquinone and a catalyst p-methylbenzenesulfonic acid, and reacting at 100-140 DEG C for 2-8 hours under the catalytic action of acid to generate a high-carbon alcohol methacrylate crude product; (2) neutralizing the high-carbon alcohol methacrylate crude product obtained in the step (1) with alkali liquor until the pH value is 7, separating the organic layer, and dehydrating at 80-150 DEG C for 1-8 hours to obtain the high-carbon alcohol methacrylate; and (3) adding acid anhydride or ester and an initiator benzoperoxide into the high-carbon alcohol methacrylate obtained in the step (2), and reacting at 70-130 DEG C for 5-10 hours to obtain the polymer. The condensation point reducer provided by the invention has dual functions of reducing both condensation point and turbidity point of the base oil, thereby eliminating the hidden danger of flammability and explosiveness.
Owner:烟台市牟平区留德润滑油销售有限公司

Method for recovering polyether from waste metal processing liquid and application of polyether in concrete slump retaining agent

The invention discloses a method for recovering polyether from waste metal processing liquid and application of the polyether in concrete slump retaining agent. The method for recovering the polyether from the waste metal processing liquid comprises the following steps: adding inorganic base to water-based waste metal processing liquid containing the polyether to adjust the pH value of the waste metal processing liquid to 10-12, standing the waste metal processing liquid for reaction, filtering, adding activated carbon and an inorganic acid to adjust the pH value of the waste metal processing liquid, heating to the temperature above the cloud point temperature, layering solution, standing at constant temperature, taking polyether phase on the upper layer, adding anti-oxidant to the polyether phase, and fully drying to remove water until the water content is 0.05 percent by weight or less to obtain the reaction product which is polyether. The following raw materials are needed when the polyether is applied to the concrete slump retaining agent: a catalyst, maleic anhydride, water, sulfonated styrene and an initiator in addition to the polyether. The polyether and the maleic anhydride are directly subjected to the esterification reaction under the heating condition without adding organic solvent and water and adopting a condensing and refluxing device, thus the equipment requirement and the production cost are reduced, and the production safety is improved. The prepared concrete slump retaining agent has good slump retaining performance, high water reducing rate and good compatibility with cement.
Owner:HOHAI UNIV +1

Biodiesel with low temperature liquidity and preparation method of biodiesel

The invention discloses a biodiesel with low temperature liquidity and a preparation method of the biodiesel. The biodiesel with low temperature liquidity comprises 2.5-30 percent by volume of direct coal liquefaction hydro-upgraded modified full-fraction oil and 70-97.5 percent by volume of illegal cooling oil biodiesel. The preparation method of the biodiesel comprises the step: after mixing the illegal cooking oil biodiesel and the direct coal liquefaction hydro-upgraded modified full-fraction oil, and standing for 8-12 hours to obtain the biodiesel with low-temperature liquidity. According to the biodiesel with low temperature liquidity, the pour point, the cloud point, the flash point, the kinematic viscosity, the oxidation stability, the heat value, the density and the acid value of mixed oil are detected according to the GB_T20828-2007, and accord with relevant requirements of EN14214 and ASTMD6751 for the technical performance of the biodiesel through detection. Compared with the illegal cooking oil biodiesel, the biodiesel has the advantages that the cloud point is reduced by 1-8 DEG C, the pour point is reduced by 2-10 DEG C, namely, the low temperature liquidity is remarkably improved, and the preparation method is simple and effective.
Owner:SHANGHAI APPLIED TECHNOLOGIES COLLEGE

Low-temperature degreaser for chemical fiber fabrics and preparation method of low-temperature degreaser

The invention discloses a low-temperature degreaser for chemical fiber fabrics and a preparation method of the low-temperature degreaser. The low-temperature degreaser is prepared from the componentsin parts by weight: 30-40 parts of fatty alcohol-polyoxyethylene ether containing alkyl polyglucoside (APG), 20-30 parts of fatty alcohol-polyoxyethylene ether phosphate containing APG, 20-30 parts offatty alcohol-polyoxyethylene ether sulphonate containing APG, 5-15 parts of a greasy dirt dispersant, 5-15 parts of a builder, 0.2-1.0 part of a pH value regulator and 30-50 parts of soft water, wherein the fatty alcohol-polyoxyethylene ether containing the APG, the fatty alcohol-polyoxyethylene ether phosphate containing the APG and the fatty alcohol-polyoxyethylene ether sulphonate containingthe APG are three main components of the low-temperature degreaser, and the proportion of the three components can be changed. Alcohol ether in a structure of the fatty alcohol-polyoxyethylene ether containing the APG has good decontaminability, degreasing performance and dispersity, the APG in the structure has the outstanding characteristic of good affinity to greasy dirt, thus the greasy dirt is better adsorbed, and the low-temperature degreaser is evenly dispersed in processing liquid, and is very suitable for a low-temperature degreasing process of the chemical fiber fabrics.
Owner:今冬科技(佛山)有限公司

A kind of low-permeability reservoir dewatering and locking agent and preparation method thereof

The invention discloses an oil field chemical agent used in petroleum gas oil-pumping operation construction, and particularly relates to a low-permeability reservoir water-lock releasing agent used in working fluid and a preparation method thereof. The low-permeability reservoir water-lock releasing agent consists of the following components in percentage by weight: 1 to 15 percent of glycol ether, 15 to 45 percent of didodecyl dicarboxylic sodium, 15 to 30 percent of ethylene glycol silicon ether and 30 to 60 percent of water. The preparation method comprises the following steps of: adding 30 to 60 percent of water into an enamel reaction kettle, starting a stirrer, and heating to raise the temperature to be between 30 and 40 DEG C; adding 1 to 15 percent of glycol ether and 15 to 45 percent of didodecyl dicarboxylic sodium into the reaction kettle, controlling the temperature and stirring for 1 hour; and adding 15 to 30 percent of ethylene glycol silicon ether into the reaction kettle, controlling the temperature to be between 40 and 80 DEG C, and reacting for 1 to 2 hours to obtain the water-lock releasing agent. The water-lock releasing agent is strong in surface activity and low in use level, can well maintain the permeability of a low-permeability reservoir and release water-lock damages, and is used in the working fluid such as fracturing fluid, perforating fluid, well control fluid and the like.
Owner:唐山冀油瑞丰化工有限公司 +1

Method for preparing biodiesel

The invention relates to the technical field of environmental engineering, oil chemistry and renewable energy sources, in particular to a method for preparing biodiesel. The method disclosed in the invention comprises the following steps of: conveying fatty acid and an oxidizing agent into a tubular hydrothermal reactor for carrying out selective oxidization treatment on the fatty acid to ensure that unsaturated bonds in the unsaturated fatty acid break to generate micromolecular saturated fatty acid; controlling the reaction conditions that the addition quantity of the oxidizing agent is 1-10 percent of oxygen quantity required for completing oxidizing raw material oil fat into CO2 and H2O, the temperature is 200-350 DEG C, the pressure is 5-30MPa, and the reaction time is 0.5-10min; directly mixing low carbon alcohol with micromolecular saturated fatty acid obtained from the step 1 for esterification to generate high-quality biodiesel with good low-temperature fluidity and strong anti-oxidization resistance; and controlling the reaction conditions that the temperature is 300-400 DEG C, the pressure is 20-35 MPa, the reaction time is 12-30min and the addition quantity of the lower carbon alcohol is 6-40 times that of the fatty acid. According to the method provided by the invention, the low-temperature fluidity and the anti-oxidization property of the biodiesel can be improved.
Owner:TONGJI UNIV
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