A kind of low-permeability reservoir dewatering and locking agent and preparation method thereof
A water-blocking agent and low-permeability technology, applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve the problem of limited application range, difficult to take into account low-permeability reservoir geology, reservoir conditions and construction techniques, and release water-locking damage Unsatisfactory effect and other problems, to achieve the effect of wide application range, release of water lock damage, and strong surface activity
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Embodiment 1
[0012] This example discloses a low-permeability oil reservoir dewatering and locking agent and its preparation method. The low-permeability oil reservoir dewatering and locking agent is composed of 50 g ethylene glycol butyl ether, 90 g N,N'-bis(dodecane Base) sodium ethylenediaminodipropionate, 70g ethylene glycol triethylsilyl ether, 160g distilled water. The specific preparation method is:
[0013] In a four-necked 500ml flask with a reflux condenser, a thermometer, and a dropping funnel, add 160g of distilled water, put a stirring magnet, put the flask into a magnetic stirrer with an electric heating jacket, turn on the magnetic stirrer, turn on the heating switch, and the temperature Control at 30-40°C, turn on the cooling water of the reflux condenser; add 50 g of ethylene glycol butyl ether, then add 90 g of N,N'-bis(dodecyl)ethylenediaminodipropionate, and react for 1 hour . Add 70g of ethylene glycol triethylsilyl ether, control the temperature at 70-80°C, and reac...
Embodiment 2
[0015] This embodiment discloses a low-permeability oil reservoir dewatering and locking agent and a preparation method thereof. By mass, this low-permeability oil reservoir dehydrating and locking agent is prepared by adding 50 g of polyethylene glycol methyl ether, 115 g of N,N'-di(dodecyl Alkyl) sodium ethylenediaminodiacetate, 56g ethylene glycol trimethylsilyl ether, 140g distilled water. The specific preparation method is:
[0016] In a four-necked 500ml flask with a reflux condenser, a thermometer, and a dropping funnel, add 140g of distilled water, put a stirring magnet, put the flask into a magnetic stirrer with an electric heating jacket, turn on the magnetic stirrer, turn on the heating switch, and the temperature Control at 30-40°C, turn on the cooling water of the reflux condenser; add 50 g of polyethylene glycol methyl ether, then add 115 g of N,N'-bis(dodecyl)ethylenediaminodiacetate, and react for 1 hour . Add 56g of ethylene glycol trimethylsilyl ether, cont...
Embodiment 3
[0018] This embodiment discloses a low-permeability oil reservoir dewatering and locking agent and a preparation method thereof. By mass, this low-permeability oil reservoir dehydrating and locking agent consists of 35 g diethylene glycol ether, 80 g N,N'-bis(dodecyl ) butanediaminodipropionate sodium, 75g polyethylene glycol trimethylsilyl ether, and 150g distilled water. The specific preparation method is:
[0019] In a four-necked 500ml flask with a reflux condenser, a thermometer, and a dropping funnel, add 150g of distilled water, put a stirring magnet, put the flask into a magnetic stirrer with an electric heating jacket, turn on the magnetic stirrer, turn on the heating switch, and the temperature Control at 30-40°C, turn on the cooling water of the reflux condenser; add 35 g of diethylene glycol ether, then add 80 g of N·Nˊ-dodecyl-ethylenediamine dipropionate, and react for 1 hour. Add 75g of polyethylene glycol trimethylsilyl ether, control the temperature at 65-75°...
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