Composition for preparing sponge powder puff and preparation method of composition

A composition and powder puff technology, which is applied to cosmetic powder containers, applications, household utensils and other directions, can solve the problems of complex raw materials and processes, environmental protection effects, etc., and achieve the effects of simple preparation method, easy operation, and fine and uniform cells.

Active Publication Date: 2014-06-04
SHANDONG INOV POLYURETHANE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] There are many patent reports based on puff appearance design, and the design ideas are also various, but there are few reports on the preparation of puff raw materials. Patent CN100391382C reports a raw material formula and production method that can be used for the preparation of multi-color puffs. Rubber latex is the main raw material, and various additives and processes required for rubber formula design are used to make puff materials. The raw materials and processes are relatively complicated. At the same time, due to the use of more chemical additives in the formula, the environmental protection will be affected.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] Prepolymer component: Weigh ethylene oxide-propylene oxide copolyether polyol DGL-8000 (customized by Bluestar Dongda Company, with 50% ethylene oxide content, 8000 molecular weight, and 3 average functionality) 70g, polytetrahydrofuran ether polyol PTMG2000, BASF product, molecular weight 2000, average functionality 2) 30g, 1,4-butanediol 3g, placed in a reaction kettle, heated to 105°C under vacuum (-0.09MPa) Dehydrate for 1.5 hours, then cool down to 45°C, add 30g of toluene diisocyanate (TDI), slowly raise the temperature to 80°C within 30 minutes, keep the temperature for 2.5 hours, take samples for detection, the mass content of -NCO is 7.0%, cool down to 50°C and discharge , sealed and preserved.

[0027] Foaming agent components: Weigh 1.0g of silicone oil DC6070 and add it to 100g of distilled water, stir evenly, and seal it for storage.

[0028] Weigh 100g of the prepolymer component and 70g of the blowing agent component, mix them quickly and evenly, pour th...

Embodiment 2

[0030] Prepolymer components: Weigh ethylene oxide-propylene oxide copolyether polyol DGL-800080g, ethylene oxide-propylene oxide copolyether polyol DEL-5000 (customized by Bluestar Dongda Company, ethylene oxide The content of alkane is 80%, the molecular weight is 5000, the average functionality is 2) 20g, and diethylene glycol is 4g, placed in a reaction kettle, heated to 100°C and dehydrated under vacuum (-0.09MPa) for 1.5 hours, and then cooled to 45°C , add 28g of toluene diisocyanate (TDI), slowly raise the temperature to 80°C within 40min, keep the temperature for 2.5 hours, take a sample for detection, the mass content of -NCO is 6.5%, cool down to 50°C and discharge, sealed and stored.

[0031] Foaming agent components: Weigh 1.5g of silicone oil AK7703 and add it to 100g of distilled water, stir evenly, and seal it for storage.

[0032] Weigh 100g of the prepolymer component and 90g of the blowing agent component and quickly mix them evenly, pour them into a mold, a...

Embodiment 3

[0034] Prepolymer components: Weigh 100g of polyether polyol DGL-8000 (customized by Bluestar Dongda Co., Ltd.), 5g of dipropylene glycol, put them in a reaction kettle, heat up to 100°C and dehydrate under vacuum (-0.09MPa) for 1.5 Hours, then lower the temperature to 50°C, add 26g of toluene diisocyanate (TDI), slowly heat up to 65°C within 20min, keep the temperature for 2.0 hours, take samples for detection, the mass content of -NCO is 6.0%, cool to 50°C and discharge, seal save.

[0035] Foaming agent components: Weigh 0.5g of silicone oil Y-10366 and add it to 100g of distilled water, stir evenly, and seal it for storage.

[0036] Weigh 100g of the prepolymer component and 50g of the blowing agent component and quickly mix them evenly, pour them into a mold, and mature for 3 minutes to obtain the sponge puff material.

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Abstract

The invention belongs to the field of polymer synthesis and particularly relates to a composition for preparing sponge powder puff and a preparation method of the composition. The composition consists of prepolymer ingredients and foaming agent ingredients according to a mass ratio being 100:(50-100), wherein the prepolymer ingredients are prepared from polyether polyol, reaction type hardening agents and toluene di-isocyanate through reaction, NCO is 5.5 to 7.0 percent, and the foaming agent ingredients consist of distilled water and organic silicon surfactants. The preparation method comprises the steps that the polyether polyol and the reaction type hardening agents are placed in a reaction kettle for dehydration, the temperature reduction is carried out, toluene di-isocyanate is added, the temperature rise reaction is carried out, and materials are discharged and are stored in a sealed way; the distilled water and the organic silicon surfactants are mixed, the uniform stirring is carried out, and the mixture is stored in a sealed way; and the prepolymer ingredients and the foaming agent ingredients are uniformly mixed and are cast into a mold for curing, and products are obtained. The sponge powder puff prepared by the composition has the advantages that excellent hydrophily and the hand feeling comfort are realized, the bubble holes are fine, dense and uniform, the powder affinity performance is high, and the use is convenient. The preparation method is simple, and the operation is easy.

Description

technical field [0001] The invention belongs to the field of polymer synthesis, and in particular relates to a composition for preparing a sponge puff and a preparation method thereof. Background technique [0002] Powder puff is one of the cosmetic products that people often use in modern society. It is not only small and beautiful, but also easy to use. It is especially favored by modern women and has almost become their daily necessities. The preparation materials of powder puff are also various, can adopt various materials such as cotton, rubber latex, foamed plastics, and different materials have respective different characteristics. [0003] The design form of the puff has a great influence on its performance, so most of the patents are also aimed at how to improve the design form to increase the usability. Patent CN201445080U reports a design and preparation method of a rolling powder puff. By adding a handle and a roller, it breaks through the form limitation of the...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08G18/76C08G18/66C08G18/48C08J9/08C08J9/00A45D33/34
Inventor 孙清峰孙兆任罗杰梁玲
Owner SHANDONG INOV POLYURETHANE
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