Composition for preparing sponge powder puff and preparation method of composition
A composition and powder puff technology, which is applied to cosmetic powder containers, applications, household utensils and other directions, can solve the problems of complex raw materials and processes, environmental protection effects, etc., and achieve the effects of simple preparation method, easy operation, and fine and uniform cells.
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Embodiment 1
[0026] Prepolymer component: Weigh ethylene oxide-propylene oxide copolyether polyol DGL-8000 (customized by Bluestar Dongda Company, with 50% ethylene oxide content, 8000 molecular weight, and 3 average functionality) 70g, polytetrahydrofuran ether polyol PTMG2000, BASF product, molecular weight 2000, average functionality 2) 30g, 1,4-butanediol 3g, placed in a reaction kettle, heated to 105°C under vacuum (-0.09MPa) Dehydrate for 1.5 hours, then cool down to 45°C, add 30g of toluene diisocyanate (TDI), slowly raise the temperature to 80°C within 30 minutes, keep the temperature for 2.5 hours, take samples for detection, the mass content of -NCO is 7.0%, cool down to 50°C and discharge , sealed and preserved.
[0027] Foaming agent components: Weigh 1.0g of silicone oil DC6070 and add it to 100g of distilled water, stir evenly, and seal it for storage.
[0028] Weigh 100g of the prepolymer component and 70g of the blowing agent component, mix them quickly and evenly, pour th...
Embodiment 2
[0030] Prepolymer components: Weigh ethylene oxide-propylene oxide copolyether polyol DGL-800080g, ethylene oxide-propylene oxide copolyether polyol DEL-5000 (customized by Bluestar Dongda Company, ethylene oxide The content of alkane is 80%, the molecular weight is 5000, the average functionality is 2) 20g, and diethylene glycol is 4g, placed in a reaction kettle, heated to 100°C and dehydrated under vacuum (-0.09MPa) for 1.5 hours, and then cooled to 45°C , add 28g of toluene diisocyanate (TDI), slowly raise the temperature to 80°C within 40min, keep the temperature for 2.5 hours, take a sample for detection, the mass content of -NCO is 6.5%, cool down to 50°C and discharge, sealed and stored.
[0031] Foaming agent components: Weigh 1.5g of silicone oil AK7703 and add it to 100g of distilled water, stir evenly, and seal it for storage.
[0032] Weigh 100g of the prepolymer component and 90g of the blowing agent component and quickly mix them evenly, pour them into a mold, a...
Embodiment 3
[0034] Prepolymer components: Weigh 100g of polyether polyol DGL-8000 (customized by Bluestar Dongda Co., Ltd.), 5g of dipropylene glycol, put them in a reaction kettle, heat up to 100°C and dehydrate under vacuum (-0.09MPa) for 1.5 Hours, then lower the temperature to 50°C, add 26g of toluene diisocyanate (TDI), slowly heat up to 65°C within 20min, keep the temperature for 2.0 hours, take samples for detection, the mass content of -NCO is 6.0%, cool to 50°C and discharge, seal save.
[0035] Foaming agent components: Weigh 0.5g of silicone oil Y-10366 and add it to 100g of distilled water, stir evenly, and seal it for storage.
[0036] Weigh 100g of the prepolymer component and 50g of the blowing agent component and quickly mix them evenly, pour them into a mold, and mature for 3 minutes to obtain the sponge puff material.
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