A kind of preparation method of sodium polyacrylate-halloysite-konjac glucomannan composite humidity-conditioning agent
A technology of konjac glucomannan and sodium polyacrylate, which is applied to the preparation of high-performance sodium polyacrylate-halloysite-konjac glucomannan composite humidity-regulating agent, and the humidity adjustment of cultural relics preservation environment. In the field, it can solve the problems of insufficient number of pores and insufficient specific surface area, etc., to achieve large specific surface area, improve humidity control performance, and good humidity stability
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Embodiment 1
[0014] Embodiment 1: a kind of preparation method of sodium polyacrylate-halloysite-konjac glucomannan composite humidity-conditioning agent, it is characterized in that the steps are as follows:
[0015] a. activating halloysite at 450° C. for 2 hours to obtain activated halloysite;
[0016] b. Take 30 parts of polyacrylic acid in parts by mass, add to 115 parts of sodium hydroxide solution (dissolve 15 parts of sodium hydroxide in 100 parts of distilled water) for neutralization, and then take 0.9 parts of konjac glucomannan in parts by mass Sugar, 3 parts of activated halloysite, 0.01 part of nanometer silver-loaded antibacterial powder, 0.3 part of potassium persulfate, 0.2 part of N,N'-methylenebisacrylamide, prepared by 0.3 part of aluminum chloride and 10 parts of water Add the aluminum chloride solution formed into the reactor containing the above-mentioned neutralized solution (the solution obtained after the neutralization of polyacrylic acid and sodium hydroxide sol...
Embodiment 2
[0019] Embodiment 2: a kind of preparation method of sodium polyacrylate-halloysite-konjac glucomannan composite humidity-conditioning agent, it is characterized in that the steps are as follows:
[0020] a. activating halloysite at 450°C for 2.5 hours to obtain activated halloysite;
[0021] b. Take 30 parts of polyacrylic acid in parts by mass, add 115 parts of sodium hydroxide solution (dissolve 15 parts of sodium hydroxide in 100 parts of distilled water) for neutralization, and then take 1.8 parts of konjac glucomannan in parts by mass Sugar, 4.5 parts of activated halloysite, 0.5 part of nanometer silver-loaded antibacterial powder, 0.3 part of potassium persulfate, 0.3 part of N,N'-methylenebisacrylamide, formulated by 0.9 part of aluminum chloride and 10 parts of water Add the aluminum chloride solution formed into the reactor containing the above-mentioned neutralized solution (the solution obtained after the neutralization of polyacrylic acid and sodium hydroxide sol...
Embodiment 3
[0024] Embodiment 3: a kind of preparation method of sodium polyacrylate-halloysite-konjac glucomannan composite humidity-conditioning agent, it is characterized in that the steps are as follows:
[0025] a. activating halloysite at 450° C. for 3 hours to obtain activated halloysite;
[0026] b. Take 30 parts by mass of polyacrylic acid, add 115 parts of sodium hydroxide solution (dissolve 15 parts of sodium hydroxide in 100 parts of distilled water) for neutralization, and then take 2.7 parts by mass of konjac glucomannan Sugar, 6 parts of activated halloysite, 1 part of nanometer silver-loaded antibacterial powder, 0.3 part of potassium persulfate, 0.4 part of N,N'-methylenebisacrylamide, prepared by 1.5 parts of aluminum chloride and 10 parts of water The formed aluminum chloride solution was added to the reactor filled with the above-mentioned neutralized solution (the solution obtained after neutralization of polyacrylic acid and sodium hydroxide solution), and stirred an...
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