Chloroethylene-isooctyl acrylate copolymer emulsion and preparation method thereof
A technology of isooctyl acrylate and copolymer emulsion, applied in application, coating, ink and other directions, can solve the problems of chemical reaction, no durability, easy to fall off, etc., achieve low cost, good waterproof and acid and alkali salt corrosion resistance , Good wear resistance and scratch resistance
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Embodiment 1
[0016] The preparation method of described vinyl chloride-isooctyl acrylate copolymer emulsion, the steps are as follows:
[0017] (1) Monomer pre-emulsification: Weigh 70 parts of vinyl chloride, 15 parts of isooctyl acrylate, and 0.5 parts of emulsifier OP-4, stir and emulsify in a pre-emulsification polymerization reactor for 1 hour, and obtain an emulsified monomer solution for later use;
[0018] (2) Preparation and addition of additives: Take 60 parts of deionized water, 2 parts of reactive emulsifier allyl nonylphenol polyvinyl ether ammonium sulfate, and 0.5 parts of sodium lauryl sulfate, stir and dissolve, then add the step ( 1) In the pre-emulsification polymerization reactor; take 1 part of the initiator ammonium persulfate and dissolve it in 20 parts of water for later use;
[0019] (3) Reaction: by volume, first take 1 / 5 of the pre-emulsified monomer in step (1) into the kettle, then add 1 / 4 of the dissolved initiator ammonium persulfate in step (2), stir for 30 ...
Embodiment 2
[0023] The preparation method of described vinyl chloride-isooctyl acrylate copolymer emulsion, the steps are as follows:
[0024] (1) Monomer pre-emulsification: Weigh 85 parts of vinyl chloride, 30 parts of isooctyl acrylate, and 3 parts of emulsifier OP-4, stir and emulsify in the pre-emulsification polymerization reactor for 2 hours, and obtain the emulsified monomer solution for later use;
[0025] (2) Preparation and addition of additives: Take 80 parts of deionized water, 5 parts of reactive emulsifier allyl nonylphenol polyvinyl ether ammonium sulfate, and 1.5 parts of sodium lauryl sulfate, and add them after fully stirring and dissolving ( 1) In the pre-emulsification polymerization reactor; take 3 parts of the initiator ammonium persulfate and dissolve it in 40 parts of water for later use;
[0026] (3) Reaction: by volume, first take 1 / 4 of the pre-emulsified monomer in step (1) into the kettle, then add 1 / 4 of the dissolved initiator ammonium persulfate in step (2...
Embodiment 3
[0030] The preparation method of described vinyl chloride-isooctyl acrylate copolymer emulsion, the steps are as follows:
[0031] (1) Monomer pre-emulsification: Weigh 80 parts of vinyl chloride, 20 parts of isooctyl acrylate, and 2 parts of emulsifier OP-4, stir and emulsify in the pre-emulsification polymerization reactor for 1 hour, and obtain the emulsified monomer solution for later use;
[0032] (2) Preparation and addition of additives: Take 70 parts of deionized water, 4 parts of reactive emulsifier allyl nonylphenol polyvinyl ether ammonium sulfate, and 1.5 parts of sodium lauryl sulfate, and add them after fully stirring and dissolving ( 1) In the pre-emulsification polymerization reactor; take 2 parts of the initiator ammonium persulfate and dissolve it in 30 parts of water for later use;
[0033] (3) Reaction: by volume, first take 1 / 5 of the pre-emulsified monomer in step (1) into the kettle, then add 1 / 3 of the dissolved initiator ammonium persulfate in step (2)...
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