Iron rust conversion agent and preparation method thereof
A conversion agent and rust technology, applied in the coating process of metal materials, etc., can solve problems such as uneven coating, poor rust conversion ability, powdering, etc.
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Embodiment 1
[0010] Preparation of component 1: Weigh 25.5kg of styrene, 20kg of butyl acrylate, and 1.5kg of methacrylic acid, put them into the reaction kettle, add 0.13kg of OP-10 emulsifier, 0.3kg of sodium lauryl sulfate, N - 1.5 kg of methylol acrylamide, 1 kg of ammonium persulfate, 30 kg of deionized water, and stirred for 20 minutes to prepare a pre-emulsion. Add 40kg of water into a three-port reaction kettle with a dropping funnel, reflux condenser, and electric stirrer, put it in a water bath and heat it. When the temperature is 80°C, add 0.4kg of OP-10 emulsifier, dodecyl 0.2kg of sodium sulfate and 0.2kg of ammonium persulfate were stirred and reacted for about 25 minutes. When the temperature of the base material is raised to 85°C, the pre-emulsion is added dropwise. The speed of the dropwise addition is slow at first and then fast. The drop is completed within 30 minutes, and the heat preservation reaction is 1-1.5h. Cool to 40°C and discharge.
[0011] Preparation of Com...
Embodiment 2
[0014] The preparation of component one is the same as in embodiment one.
[0015] Preparation of Component 2: At room temperature, add 8 kg of distilled water and 8 kg of absolute ethanol to a reaction kettle with a stirring device, start stirring, add 2.5 kg of pyrogallic acid and 1 kg of tannic acid in sequence until completely dissolved, and stir State, continue to add 2kg citric acid, 1kg isopropanol until completely dissolved.
[0016] Preparation of rust conversion agent: accurately weigh 70kg of component 1, add 4.9kg of film-forming aids, stir well, add 25kg of component 1, 0.1kg of simethicone, and stir for 20min until the system is uniform.
Embodiment 3
[0018] The preparation of component one is the same as in embodiment one.
[0019] Preparation of Component 2: At room temperature, add 6kg of distilled water and 6kg of absolute ethanol to a reaction kettle with a stirring device, start stirring, add 1kg of pyrogallic acid and 2.5kg of tannic acid in sequence until completely dissolved, and stir State, continue to add 1.5kg citric acid, 1.5kg isopropanol until fully dissolved.
[0020] Preparation of rust conversion agent: accurately weigh 63kg of component 1, add 5.3kg of film-forming aid, and stir well, then add 31.5kg of component 1 and 0.2kg of simethicone, and stir for 20 minutes until the system is uniform.
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