Hydrophilic aminosilicon oil, and preparation method and uses thereof

A technology of amino silicone oil and hydrophilic type, which is applied in the direction of fiber type, textile and paper making, fiber treatment, etc. It can solve the problems of reducing whiteness, poor antistatic property, and discoloration.

Active Publication Date: 2013-07-10
安徽科光新材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, the silicone oils that are widely used in the market have many shortcomings such as yellowing of plants, discoloration, reduction of whiteness, poor stability, moisture absorption (perspiration) and antistatic properties of easy-to-stain fabrics, so in order to keep up with the market needs and application conditions, the existing technology needs to be updated and improved

Method used

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  • Hydrophilic aminosilicon oil, and preparation method and uses thereof
  • Hydrophilic aminosilicon oil, and preparation method and uses thereof
  • Hydrophilic aminosilicon oil, and preparation method and uses thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] Add high hydrogen-containing silicone oil, D4, hexamethyldisilazane, and ammonia water in a ratio of 10:1:1.5:1 to the mouth of a three-necked flask equipped with a stirrer, a reflux condenser, and a thermometer, stir, and heat up to 80 After reacting at ℃ for 3 hours, add sulfamic acid, continue to stir for 2 hours, and then carry out suction filtration, distillation, and removal of low boilers to obtain low-hydrogen silicone oil with an appropriate hydrogen content;

[0032] Add low-hydrogen silicone oil and D4 into the reaction kettle equipped with a stirrer, reflux condenser and thermometer in sequence at a ratio of 10:0.15, and pass N 2 Stir and heat up to 60°C, add zinc oxide, continue to stir, and react at a constant temperature of 110°C for 3 hours, the reaction solution becomes turbid and clear;

[0033] Then add methyltriethoxysilane and allyl polypropylene glycol into the reaction kettle in sequence at 1:10, keep the material reaction until transparent at 110...

Embodiment 2

[0042] Add high hydrogen-containing silicone oil, DMC, hexamethyldisilazane, and ammonia water in a ratio of 10:1:1.5:1 into the mouth of a three-necked flask equipped with a stirrer, reflux condenser, and thermometer, stir, and heat up to 80°C React for 3 hours, add neutralizing agent with zinc oxide, continue to stir for 2 hours, carry out suction filtration, distillation, and remove low boilers to obtain low hydrogen silicone oil with proper hydrogen content;

[0043] Add low-hydrogen silicone oil and D4 into the reaction kettle equipped with a stirrer, reflux condenser and thermometer in sequence at a ratio of 10:0.3, and stir with N2. After the temperature rises to 60°C, add heavy metal oxides, continue to stir, and react at a constant temperature of 110°C. After 3 hours, the reaction solution became turbid and clear;

[0044] Then add methyltriethoxysilane and allyl polypropylene glycol into the reaction kettle in sequence at 0.5:10, keep the material reaction until tran...

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Abstract

The invention relates to a hydrophilic aminosilicon oil, and a preparation method and uses thereof. The preparation method comprises the following steps: carrying out an addition reaction of hydrogen-containing silicon oil and a methoxy-group-containing compound in the presence of a catalyst to prepare epoxy modified silicon oil, and carrying out a quaternary copolymerization addition reaction of the epoxy modified silicon oil, an amino compound, a silane coupling agent and polyether to prepare the novel hydrophilic aminosilicon oil. When the hydrophilic aminosilicon oil is used for finishing polyester and pure terylene fabrics, excellent soft and smooth hand feelings are obtained, and the hydrophilicity, the moisture (sweat) absorption property and the antistatic performance of the fabrics are improved; and the performances of the hydrophilic aminosilicon oil are better than that of hydrophilic aminosilicon oil sold in the market at present, so the hydrophilic aminosilicon oil prepared in the invention has a broad market prospect.

Description

technical field [0001] The invention relates to the field of fabric softening and finishing agents, in particular to a hydrophilic amino silicone oil and its preparation method and application. Background technique [0002] People's requirements for clothing are not simply to require fabrics to be hygroscopic, breathable, and comfortable to wear, but also to pursue soft, smooth, and elegant styles of fabrics. Therefore, softeners appear, and the most widely used ones today are Silicone softener. Silicone softeners were first researched, developed and applied in European and American countries, and made huge profits. Since the reform and opening up, my country's economy has developed rapidly, and the textile printing and dyeing industry has developed from the use of silicone softeners to the gradual application, and now it is fully applied. my country has joined the WTO for many years, and the most competitive industrial products in the international market are textile prod...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08G77/388D06M15/647D06M101/06D06M101/32
Inventor 王绪荣陈必连楚大生王晓红周军昌韦永方梁健殷彬励欧阳磊王肖俊
Owner 安徽科光新材料有限公司
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