Application of organosilicon-modified high-molecular compound as seed coating film-forming agent
A high molecular compound and organosilicon technology, which is applied in the direction of seed coating/seed dressing, application, animal repellent, etc., can solve the problems of complex processing technology, poor stability, poor water permeability, etc., and achieve strong compatibility and weather resistance Excellent performance and improved air permeability
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Example Embodiment
[0065] Example 1
[0066] In a four-necked flask with stirring, add 0.5 parts of vinyl trimethoxysilane, 5 parts of octamethylcyclotetrasiloxane, 1.5 parts of 99% acrylamide, 1 part of acrylic acid, 0.1 part of ammonium persulfate, 5 parts of butyl acrylate, 1 part of acrylonitrile, 0.2 part of sodium dodecylbenzene sulfonate, 0.1 part of N,N,N',N'-tetramethylethylenediamine, 750 parts of deionized water, add each After the raw materials, quickly stir for 30 minutes, and then heat to 75°C-80°C. After 3 hours of heat preservation and reaction, stop heating, cool to room temperature, adjust the pH value with ammonia water, and stir evenly to discharge. Obtained viscous transparent liquid, its pH value is 6.8, the viscosity at room temperature is 1900mPaS, the viscosity average molecular weight is 750,000, m≈2000, n≈1060, and the structural formula is
[0067]
[0068] X is the group shown below:
[0069]
[0070] R 1 , R 2 , R 3 Is hydrogen;
[0071] R 4 , R 5 , R 6 , R 7 Is methoxy; ...
Example Embodiment
[0073] Example 2
[0074] In a four-necked flask with stirring, add 0.5 parts of vinyltrimethoxysilane, 5 parts of octamethylcyclotetrasiloxane, 1.3 parts of 99% acrylamide, 1 part of acrylic acid, 0.2 parts of ammonium persulfate, 5 parts of butyl acrylate, 1 part of methyl methacrylate, 0.1 part of sodium dodecylbenzene sulfonate, 0.1 part of N,N,N',N'-tetramethylethylenediamine, 125 parts of deionized water, After adding each raw material, stir quickly for 30 minutes, then heat to 75°C-80°C, after keeping the temperature for 3 hours, stop heating, cool to room temperature, adjust the pH value with ammonia water, and stir evenly to discharge. Obtained viscous transparent liquid, its pH value is 6.8, the viscosity is 1750mPaS at room temperature, the viscosity average molecular weight is 625,000, m≈1810, n≈1030, and the structural formula is:
[0075]
[0076] X is the group shown below:
[0077]
[0078] R 1 , R 2 , R 3 Is hydrogen;
[0079] R 4 , R 5 , R 6 , R 7 Is methoxy;
[008...
Example Embodiment
[0081] Example 3
[0082] In a four-necked flask with stirring, add 0.5 parts of vinyl triethoxy silane, 5 parts of tetramethyl tetravinyl cyclotetrasiloxane, and then add 1 part of 99% acrylamide, 1 part of acrylic acid, and persulfuric acid. 0.1 part of ammonium, 5 parts of N-vinylpyrrolidone, 1 part of acrylonitrile, 0.2 part of sodium dodecylbenzene sulfonate, 0.1g of N,N,N',N'-tetramethylethylenediamine, deionized water 75 parts, after adding each raw material, quickly stir for 30 minutes, then heat to 75°C-80°C, after keeping the reaction temperature for 3 hours, stop heating, cool to room temperature, adjust the pH value with ammonia water, and stir evenly to discharge. Obtained viscous transparent liquid, its pH value is 6.8, the viscosity is 2200mPaS at normal temperature, the viscosity average molecular weight is 800,000, m≈2100, n≈1050, and the structural formula is:
[0083]
[0084] X is the group shown below:
[0085]
[0086] R 1 , R 2 , R 3 Is hydrogen;
[0087] R 4 ...
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