Ultrasonic fumigating atomization method for insect-expelling and anti-mildew for storage agricultural products by utilizing composite essential oil
A technology of ultrasonic atomization and essential oils, which is applied in application, food preservation, edible seed preservation, etc., can solve the problems of increasing operators’ exposure to toxic gases, mold and other microorganisms that are not inhibited, and endanger human health, etc. Drug resistance, low cost, good volatility
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Embodiment 1
[0046] Dehydration and refining of litsea cubeba oil, clove oil, patchouli oil and geranium oil: Litsea cubeba oil, clove oil, patchouli oil and geranium oil purchased from rural areas are directly put into w-2 batch alcohol recovery distillation tower (Wuxi LTECH Petrochemical Equipment Company) at 130 ° C, 1.15 atmospheric pressure for secondary distillation, after collection, add CaCl 2 Dehydration, so that the water content in the essential oil is less than 3%.
[0047] Preparation of cinnamon oil: buy benzaldehyde with a volume percentage above 96.1% from the market and mix glyoxylic acid at a volume ratio of 1:1.2, then add it to a reaction kettle and react at 25°C for 15 minutes, stirring at 110 times / min while adding. After standing still for 8 hours, the unreacted glyoxylic acid in the lower layer was released, and the reactant in the upper layer was cinnamon oil.
[0048] Composite essential oil preparation method: according to the volume ratio of 7:1:1:0.5:0.5, fiv...
Embodiment 2
[0052] According to attached figure 1 The design drawings and drawings of the ultrasonic fumigation and atomization device are described, and the implementation is carried out according to the connection relationship between the components in the various parts of the circuit described in the summary of the invention, and the technical parameter requirements of the components described in the implementation mode. The present invention can be practiced.
[0053] A kind of ultrasonic fumigation and atomization device, such as figure 1 As shown, the ultrasonic fumigation and atomization device includes a DC power supply 1 , connecting wires 2 , an atomization cylinder cover 3 , an atomization cylinder body 4 , an ultrasonic transducer 5 , an atomization pipeline interface 6 and a blower system 7 . The output terminal 2-1 of the connecting wire 2 is connected to the DC power supply 1, and the input terminal 2-2 of the connecting wire 2 is connected to the ultrasonic transducer 5 t...
Embodiment 3
[0067] Microscopic determination of the atomization effect: use a pipette to draw 2-3 μL of water on the cleaned glass slide, and push the water droplets away, put the ultrasonic transducer in the ultrasonic fumigation atomization device made in Example 2 into In a 2L beaker filled with compound essential oils, turn on the power supply for ultrasonic atomization, and use a glass slide coated with a water layer to collect water at a distance of 5cm, 25cm and 40cm from the atomized liquid surface (the side of the slide with fog droplets) respectively. Put the collected droplet under an inverted microscope to observe and take pictures; then use a micrometer to calibrate the droplet at the same magnification, and finally use the scnimagt software to extract the gray ratio and boundary of the image And statistical analysis, the results show that Figure 4 : 66% of the most abundant droplets are collected in the droplet samples collected at a distance of 5cm from the liquid surface....
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