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Energy-saving preparation method for high-purity baical skullcap root extract

A Scutellaria baicalensis extract and high-purity technology are applied in the field of extract preparation, which can solve the problems of high consumption, complex preparation process, environmental pollution and the like, and achieve the effects of cost saving and resource consumption reduction.

Active Publication Date: 2013-12-04
哈尔滨儿童制药厂有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] Up to now, in the reported preparation processes of Scutellaria baicalensis extract, single-effect or double-effect evaporators are mostly used in the concentration process, and the energy consumption is high; some preparation processes produce sewage without recycling, and the discharge of waste water and waste residues is large, which is harmful to the environment. Pollution; some preparation processes are complicated, the cost of extracting and separating baicalin is high, and the preparation process consumes a large amount of organic solvents such as ethanol
Some preparation processes are simple, but the product quality is unstable and cannot meet user needs

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Embodiment Construction

[0028] In order to have a clearer understanding of the technical features, purposes and effects of the present invention, the specific implementation manners of the present invention will now be described with reference to the accompanying drawings.

[0029] The present invention also provides an energy-saving preparation method of a high-purity Scutellaria baicalensis extract, comprising the following steps:

[0030] A. Clean selection treatment: take 10kg of fresh medicinal materials of Scutellaria baicalensis, remove residual stems and impurities, rinse with water, and let stand to drain the water on the surface of Scutellaria baicalensis;

[0031] B. Enzyme-inactivating slices: use the damp heat method to inactivate the enzyme-inactivated Scutellaria baicalensis, and process the inactivated Scutellaria baicalensis into 3mm thick decoction pieces;

[0032] C. Extraction and filtration: Put the slices of Scutellaria baicalensis into hot water at 95°C for extraction twice. Th...

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Abstract

The invention discloses an energy-saving preparation method for a high-purity baical skullcap root extract. The method mainly comprises the following steps: cleaning and selecting, enzyme deactivation and slicing, extraction and filtering, primary precipitation and filtering, refining and filtering, secondary precipitation and filtering, acid rinsing and drying, fusing and filtering, liquid medicine concentration, liquid medicine drying, medicine dreg processing and the like. According to the invention, a mechanical steam recompression concentration process is adopted for liquid medicine concentration; a combined drying process is adopted for liquid medicine drying; the method has the characteristics of energy conservation, consumption reduction and carbon emission reduction, as for each ton of baical skullcap root extract, 5-7 tons of standard coal is saved, 100-120 tons of waste water is processed, 80-100 tons of distilled water with the temperature of 40-50 DEG C is recycled, and the energy-saving indicator is improved by more than 30 percent. Due to the adoption of the method, zero emission of waste water and dregs of the manufacturing technology is realized; no external additive or organic menstruum is used in the extraction process of the baical skullcap root extract, and accordingly the cost is obviously saved, and the resource consumption is reduced.

Description

technical field [0001] The invention relates to a method for preparing an extract, in particular to a method for extracting substances from Scutellaria baicalensis. Background technique [0002] Scutellaria baicalensis is the dry root of Scutellaria baicalensis Georgi, a plant of the Labiatae family. It is widely distributed in my country and is produced in Heilongjiang, Jilin, Liaoning, Henan, Hebei, Shandong, Sichuan, Yunnan, Shanxi, Shaanxi, Gansu and Inner Mongolia. Scutellaria baicalensis mainly has the following functions: clearing heat and dampness, purging fire and detoxification, hemostasis, anti-abortion; it is used to treat mainly damp-warm, summer-dampness, chest tightness and nausea, damp-heat fullness, diarrhea, jaundice, lung-heat cough, high fever and polydipsia, Blood heat spits nosebleed, carbuncle sores, and fetal restlessness; Scutellaria baicalensis also has anti-inflammatory, anti-allergic, anti-microbial effects, antipyretic, antihypertensive, diuretic...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K36/539
Inventor 王增淑姚瑞东王增理
Owner 哈尔滨儿童制药厂有限公司