A kind of manufacturing process of crystalline nano pet plastic
A production process and crystallization technology, applied in the field of plastic material production technology, can solve the problems of difficult processing, poor impact resistance, slow crystallization speed of PET plastic, etc., and achieve easy processing, strong impact resistance, and ensure high purity. Effect
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Embodiment 1
[0022] A kind of manufacturing process of crystalline nano-PET plastic of the present embodiment, its processing step is as follows:
[0023] (1) Raw material preparation; under the conditions of reaction temperature 250-300°C and reaction pressure 2-2.5MPa, using zinc compound as catalyst, crude terephthalic acid is made into high-purity terephthalic acid (PTA), whichever is its purity 98%;
[0024] (2) Blending; mixing the terephthalic acid prepared in step (1) with ethylene glycol (EG), the mass ratio of the terephthalic acid to ethylene glycol (EG) is 1:1.5~2, Add CaCO to the mixed solution 3 Inorganic filler, the mass content of described filler is 3%~5%;
[0025] (3) Esterification: add a catalyst to the mixture of step (2), under the action of the catalyst, terephthalic acid and ethylene glycol undergo an esterification reaction, and the catalyst is acetate of zinc, cobalt, and manganese The mixture with antimony trioxide, the amount of the catalyst is 0.01%~0.05% of...
Embodiment 2
[0035] Example 2: The rest are the same as in Example 1, the difference is that the purity of the terephthalic acid prepared in step (1) is medium, and in this example, the cost is relatively low, but the reaction rate for making plastic is slow , the efficiency is low, and the physical properties of the plastic are reduced.
Embodiment 3
[0036]Embodiment 3: the rest are the same as the above-mentioned embodiment 1, the difference is that in the step (6), the crystallization accelerator is changed: sodium benzoate is organic montmorillonite, in this implementation, the corresponding reaction temperature increases, crystallization Effect is worse than embodiment 1.
[0037] It is known from practical application that the production of raw materials goes through six steps of preparation, blending, esterification reaction, polycondensation reaction, reinforcement modification, crystallization and separation, so that PET rubber not only has excellent physical and mechanical properties in a wide temperature range, but also has excellent electrical properties. Excellent insulation, creep resistance, fatigue resistance, friction resistance, good dimensional stability, fast crystallization rate, easy molding and processing, and strong impact resistance. Phthalic acid ensures the high purity of plastic products and impr...
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