Printing paste used for gold powder printing of stone wall paper and preparation method

A printing pulp and wallpaper technology, applied in dyeing, textiles and papermaking, etc., can solve the problems of no special products and technology disclosure, poor resistance to air oxidation, easy to lose the gorgeous luster of gold powder, etc.

Active Publication Date: 2014-04-23
LIAONING FIXED STAR FINE CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Especially for gold powder printing, the above shortcomings are more obvious, and the air oxidation resistance is not good, and it is easy to lose the go

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0030] Example 1

[0031] Raw material weight ratio:

[0032] (1) Emulsifying mixed monomer: Add 2.0 parts of 1.4 butanediol dimethacrylate, 1.0 part of itaconic acid, 130 parts of ethyl acrylate, 31 parts of butyl acrylate, and 6.4 parts of hydroxyethyl methacrylate into the stainless steel kettle. Parts, 27 parts of methyl methacrylate, 4.0 parts of acetoacetoxyethyl methacrylate, 32 parts of styrene, 2 parts of fatty alcohol polyoxyethylene ether 23E9, 210 parts of deionized water, stir to make an emulsion, To be used

[0033] (2) Initiate the polymerization reaction: take 30% of the total weight of the above-mentioned emulsion and add it to the reactor, increase the temperature to 80-82°C, add the initiator, a mixture of 1.27 parts of ammonium persulfate and 10 parts of deionized water, to initiate, then Add the remaining emulsified liquid dropwise at 80-82℃, and add 0.63 part of ammonium persulfate and 10 parts of deionized water dropwise at the same time. After 1 hour, the ...

Example Embodiment

[0035] Example 2

[0036] (1) Emulsification mixed monomer: In a stainless steel kettle, add 2.1 parts of 1.4 butanediol dimethacrylate, 1.05 parts of itaconic acid, 135 parts of ethyl acrylate, 31.5 parts of butyl acrylate, and 6.5 parts of hydroxyethyl methacrylate. Parts, 27.5 parts of methyl methacrylate, 4.1 parts of acetoacetoxyethyl methacrylate, 32.5 parts of styrene, 2.2 parts of fatty alcohol polyoxyethylene ether 23E9, 220 parts of deionized water, stir to make an emulsion, To be used

[0037] (2) Initiate the polymerization reaction: take 30% of the total weight of the above-mentioned emulsion and add it to the reactor, increase the temperature to 80-82°C, add the initiator, a mixture of 1.27 parts of ammonium persulfate and 10 parts of deionized water, to initiate, then Add the remaining emulsified liquid dropwise at 80-82℃, and add 0.73 parts of ammonium persulfate and 10 parts of deionized water dropwise at the same time. After 1.5 hours of dripping, keep at 80-82℃ ...

Example Embodiment

[0039] Example 3

[0040] (1) Emulsification mixed monomer: In a stainless steel kettle, add 2.2 parts of 1.4 butanediol dimethacrylate, 1.1 parts of itaconic acid, 140 parts of ethyl acrylate, 32 parts of butyl acrylate, and 6.6 parts of hydroxyethyl methacrylate. Parts, 28 parts of methyl methacrylate, 4.2 parts of acetoacetoxyethyl methacrylate, 33 parts of styrene, 2.3 parts of fatty alcohol polyoxyethylene ether 23E9, 230 parts of deionized water, stir to make an emulsion, To be used

[0041] (2) Initiate the polymerization reaction: take 30% of the total weight of the above-mentioned emulsion and add it to the reactor, increase the temperature to 80-82°C, add the initiator, a mixture of 1.27 parts of ammonium persulfate and 10 parts of deionized water, to initiate, then Add the remaining emulsion dropwise at 80-82℃, and at the same time add 0.83 parts of ammonium persulfate and 10 parts of deionized water. After 2 hours of dripping, keep it at 80-82℃ for 2-3 hours, then cool...

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PUM

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Abstract

The invention discloses printing paste used for gold powder printing of stone wall paper and a preparation method. The printing paste is prepared by carrying out the following steps: emulsifying 2.0-2.2 parts by mass of 1,4-butanediol dimethacrylate, 1.0-1.1 parts by mass of itaconic acid, 130-140 parts by mass of ethyl acrylate, 31-32 parts by mass of butyl acrylate, 6.4-6.6 parts by mass of hydroxyethyl methylacrylate, 27-28 parts by mass of methyl methacrylate, 4.0-4.2 parts by mass of 2-(methacryloyloxy)ethyl acetoacetate, 32-33 parts by mass of styrene, 2-2.3 parts by mass of fatty alcohol-polyoxyethylene ether 23E9 and 230-250 parts by mass of deionized water, and initiating polymerization; compounding 20-25 parts by mass of a mixed solution of sorbitol and benzotriazole, 20-22 parts by mass of an associative leveling rheological agent and 10-15 parts by mass of an acrylic dispersant, and mixing. The printing paste in high in transparency, glossiness and fastness, and is resistant to air oxidation.

Description

technical field [0001] The invention relates to a printing paste for stone wallpaper gold powder printing, that is, the printing paste used for printing gold patterns on stone wallpaper. Background technique [0002] Stone wallpaper is made of calcium carbonate as the main raw material, polymer materials and various inorganic substances as auxiliary materials. [0003] The prior art does not have special printing paste for stone wallpaper, and adhesives are used instead of printing paste, such as the adhesive IT of BASF, adding thickener, water, and printing paste to mix to make stone wallpaper printing paste. The gloss, elasticity, and hand feeling of the printed pattern are not satisfactory, and the unevenness is not strong. Especially in gold powder printing, the above shortcomings are more obvious, and the air oxidation resistance is not good, and it is easy to lose the gorgeous luster of gold powder. [0004] As for the printing paste for gold powder printing of stone...

Claims

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Application Information

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IPC IPC(8): D06P1/52D06P1/651D06P1/642D06P1/653C08F220/18C08F212/08C08F220/14C08F220/28C08F222/14C08F222/02C08F2/30
Inventor 倪成涛周明陈红梅郑文慧
Owner LIAONING FIXED STAR FINE CHEM
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