Printing paste used for gold powder printing of stone wall paper and preparation method
A printing pulp and wallpaper technology, applied in dyeing, textiles and papermaking, etc., can solve the problems of no special products and technology disclosure, poor resistance to air oxidation, easy to lose the gorgeous luster of gold powder, etc.
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Embodiment 1
[0031] Raw material weight ratio:
[0032] (1) Emulsifying mixed monomer: Add 2.0 parts of 1.4 butanediol dimethacrylate, 1.0 part of itaconic acid, 130 parts of ethyl acrylate, 31 parts of butyl acrylate, and 6.4 parts of hydroxyethyl methacrylate into the stainless steel kettle. Parts, 27 parts of methyl methacrylate, 4.0 parts of acetoacetoxyethyl methacrylate, 32 parts of styrene, 2 parts of fatty alcohol polyoxyethylene ether 23E9, 210 parts of deionized water, stir to make an emulsion, To be used
[0033] (2) Initiate the polymerization reaction: take 30% of the total weight of the above-mentioned emulsion and add it to the reactor, increase the temperature to 80-82°C, add the initiator, a mixture of 1.27 parts of ammonium persulfate and 10 parts of deionized water, to initiate, then Add the remaining emulsified liquid dropwise at 80-82℃, and add 0.63 part of ammonium persulfate and 10 parts of deionized water dropwise at the same time. After 1 hour, the dripping is complete...
Embodiment 2
[0036] (1) Emulsification mixed monomer: In a stainless steel kettle, add 2.1 parts of 1.4 butanediol dimethacrylate, 1.05 parts of itaconic acid, 135 parts of ethyl acrylate, 31.5 parts of butyl acrylate, and 6.5 parts of hydroxyethyl methacrylate. Parts, 27.5 parts of methyl methacrylate, 4.1 parts of acetoacetoxyethyl methacrylate, 32.5 parts of styrene, 2.2 parts of fatty alcohol polyoxyethylene ether 23E9, 220 parts of deionized water, stir to make an emulsion, To be used
[0037] (2) Initiate the polymerization reaction: take 30% of the total weight of the above-mentioned emulsion and add it to the reactor, increase the temperature to 80-82°C, add the initiator, a mixture of 1.27 parts of ammonium persulfate and 10 parts of deionized water, to initiate, then Add the remaining emulsified liquid dropwise at 80-82℃, and add 0.73 parts of ammonium persulfate and 10 parts of deionized water dropwise at the same time. After 1.5 hours of dripping, keep at 80-82℃ for 2-3 hours, the...
Embodiment 3
[0040] (1) Emulsification mixed monomer: In a stainless steel kettle, add 2.2 parts of 1.4 butanediol dimethacrylate, 1.1 parts of itaconic acid, 140 parts of ethyl acrylate, 32 parts of butyl acrylate, and 6.6 parts of hydroxyethyl methacrylate. Parts, 28 parts of methyl methacrylate, 4.2 parts of acetoacetoxyethyl methacrylate, 33 parts of styrene, 2.3 parts of fatty alcohol polyoxyethylene ether 23E9, 230 parts of deionized water, stir to make an emulsion, To be used
[0041] (2) Initiate the polymerization reaction: take 30% of the total weight of the above-mentioned emulsion and add it to the reactor, increase the temperature to 80-82°C, add the initiator, a mixture of 1.27 parts of ammonium persulfate and 10 parts of deionized water, to initiate, then Add the remaining emulsion dropwise at 80-82℃, and at the same time add 0.83 parts of ammonium persulfate and 10 parts of deionized water. After 2 hours of dripping, keep it at 80-82℃ for 2-3 hours, then cool down To 30-40℃, ...
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