High-performance soft magnetic ferrite for LED (light-emitting diode) lighting and display screen
A soft magnetic ferrite and LED lighting technology, applied in the field of MnZn ferrite materials and its preparation, can solve the problems of high power consumption and poor DC superposition performance, and achieve low porosity, excellent DC superposition characteristics, density high effect
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Embodiment 1
[0021] (1) Weighing: Accurately weigh 58mol% Fe 2 o 3 , 35mol% MnO (raw material is Mn 3 o 4 ), 7mol% ZnO, 2500ppm CaCO 3 , 2000ppm of Nb 2 o 5 , 1200ppm V 2 o 5 , Bi of 1000ppm 2 o 3 and 500ppm Cr 2 o 3 spare;
[0022] (2) Mixing and grinding: the weighed Fe 2 o 3 , MnO and ZnO were placed in a mixer with a rotation speed of 100 rpm and stirred for 20 minutes, and then the mixed material was placed in a vibration grinder with a vibration frequency of 80 times / min and a vibration amplitude of 3 mm for 30 minutes to obtain Mixed materials with an average particle size of 0.7 μm;
[0023] (3) Preparation of mixed slurry: add weighed CaCO to the above ground mixed material in sequence 3 , Nb 2 o 5 , V 2 o 5 、MoO 3 and Co 2 o 3 , pure water and dispersant 2.5 times the weight of the mixed material, and then grind at a speed of 70 rpm for 45 minutes to obtain a mixed solution with an average particle size of 0.65 μm, and finally add a concentration of 20% that...
Embodiment 2
[0027] (1) Weighing: Accurately weigh 54.3mol% Fe 2 o 3 , 33mol% MnO (raw material is Mn 3 o 4 ), 5.5mol% ZnO, 800ppm CaCO 3 , 500ppm of Nb 2 o 5 , 300ppm V 2 o 5 , Bi of 500ppm 2 o 3 and 300ppm Cr 2 o 3 spare;
[0028] (2) Mixing and grinding: the weighed Fe 2 o 3, MnO and ZnO were placed in a mixer with a rotating speed of 80 rpm and stirred and mixed for 20 minutes, and then the mixed material was placed in a vibration grinder with a vibration frequency of 80 times / min and a vibration amplitude of 3 mm for 30 minutes to obtain Mixed materials with an average particle size of 0.8 μm;
[0029] (3) Preparation of mixed slurry: add weighed CaCO to the above ground mixed material in sequence 3 , Nb 2 o 5 , V 2 o 5 、MoO 3 and Co 2 o 3 , pure water and dispersant 2.5 times the weight of the mixed material, and then grind at a speed of 80 rpm for 45 minutes to obtain a mixed solution with an average particle size of 0.7 μm, and finally add a concentration of 2...
Embodiment 3
[0033] (1) Weighing: Accurately weigh 56mol% Fe 2 o 3 , 34mol% MnO (raw material is Mn 3 o 4 ), 6mol% ZnO, 1500ppm CaCO 3 , 1200ppm Nb 2 o 5 , 900ppm V 2 o 5 , Bi of 800ppm 2 o 3 and 400ppm Cr 2 o 3 spare;
[0034] (2) Mixing and grinding: the weighed Fe 2 o 3 , MnO and ZnO were placed in a mixer with a rotation speed of 100 rpm and stirred and mixed for 10 minutes, and then the mixed material was placed in a vibration grinder with a vibration frequency of 80 times / min and a vibration amplitude of 3 mm for 20 minutes to obtain Mixed materials with an average particle size of 0.7 μm;
[0035] (3) Preparation of mixed slurry: add weighed CaCO to the above ground mixed material in sequence 3 , Nb 2 o 5 , V 2 o 5 、MoO 3 and Co 2 o 3 , pure water and dispersant 2.5 times the weight of the mixed material, and then grind at a speed of 60 rpm for 45 minutes to obtain a mixed solution with an average particle size of 0.6 μm, and finally add a concentration of 0.5 ...
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Abstract
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