Smelting and casting method and casting device of titanium-based amorphous composite material

An amorphous composite material, titanium-based technology, applied in the configuration of casting equipment, manufacturing tools, indicating equipment/measuring equipment, etc., can solve problems such as difficult temperature measurement, segregation of high melting point material components, and affecting casting performance, etc., to achieve simplification process, avoid pollution, and achieve the effect of filling

Active Publication Date: 2014-06-04
NORTHWESTERN POLYTECHNICAL UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, if this method is used to prepare large-scale titanium-based amorphous composite materials, there are still some unsolvable problems: firstly, the V-shaped quartz funnel where the alloy is placed will react strongly with titanium at high temperature. When the liquid is completely suspended, the composition will still be inaccurate due to the reaction; the second suspension coil has a limited suspension capacity, which limits the development of amorphous composite castings to large sizes; the third spray-casting sample There will be porosity problems, which will affect the performance of castings
However, there are certain problems with this method: firstly, it is difficult to measure the temperature by adopting the upper end suction casting mold, and the upper end suction casting mold blocks the best temperature measurement position, so it can only be realized by controlling the smelting voltage. level control, but a good correspondence cannot be established between the smelting voltage and the actual temperature of the melt; secondly, the upper-end suction casting needs to insert a long quartz tube into the melt, so this method cannot be applied to the Titanium-based amorphous composite material that reacts strongly with quartz; thirdly, heating the raw material directly in a water-cooled copper crucible will often cause the high-melting point substance to not completely melt and cause strong component segregation

Method used

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  • Smelting and casting method and casting device of titanium-based amorphous composite material
  • Smelting and casting method and casting device of titanium-based amorphous composite material
  • Smelting and casting method and casting device of titanium-based amorphous composite material

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Embodiment 1

[0057] This embodiment is a preparation method of a titanium-based amorphous composite material, and the composition of the amorphous composite material is Ti 46 Zr 20 Nb 12 Cu 5 be 15 , A rod with a diameter of Φ12mm and a length of 140mm made by suction casting in a water-cooled copper crucible. The concrete process of this embodiment is:

[0058] Step 1, smelting the alloy master ingot: Melting Ti, Zr, Nb, Cu, Be with a purity greater than 99.9% in two steps through an electric arc melting furnace under the protection of argon. The electric arc melting furnace can simultaneously melt three alloy ingots; each alloy ingot has a weight of 30 g.

[0059] The specific process of smelting alloy master ingot is:

[0060] The first step is to melt the TiZrNb alloy ingot. First, Ti, Zr, and Nb with high melting points are smelted into TiZrNb melt; the power of the arc melting furnace is turned off, and the TiZrNb melt is cooled and solidified to form a TiZrNb alloy ingot. Tu...

Embodiment 2

[0080] This embodiment is a preparation method of a titanium-based amorphous composite material, and the composition of the amorphous composite material is Ti 48 Zr 20 Nb 12 Cu 5 be 15 , A rod with a diameter of Φ12mm and a length of 140mm made by suction casting in a water-cooled copper crucible. The concrete process of this embodiment is:

[0081] Step 1, smelting the alloy master ingot: Melting Ti, Zr, Nb, Cu, Be with a purity greater than 99.9% in two steps through an electric arc melting furnace under the protection of argon. The electric arc melting furnace can simultaneously melt three alloy ingots; each alloy ingot has a weight of 30g.

[0082] The specific process of smelting alloy master ingot is:

[0083] The first step is to melt the TiZrNb alloy ingot. First, Ti, Zr, and Nb with high melting points are smelted into TiZrNb melt; the power of the arc melting furnace is turned off, and the TiZrNb melt is cooled and solidified to form a TiZrNb alloy ingot. Tur...

Embodiment 3

[0103] This embodiment is a preparation method of a titanium-based amorphous composite material, and the composition of the amorphous composite material is Ti 48 Zr 20 Nb 12 Cu 5 be 15 , a rod with a diameter of Φ12mm and a length of 30mm made by suction casting in a water-cooled copper crucible. The concrete process of this embodiment is:

[0104] Step 1, smelting the alloy master ingot: Melting Ti, Zr, Nb, Cu, Be with a purity greater than 99.9% in two steps through an electric arc melting furnace under the protection of argon. The electric arc melting furnace can simultaneously melt three alloy ingots; each alloy ingot has a weight of 30 g.

[0105] The specific process of smelting alloy master ingot is:

[0106] The first step is to melt the TiZrNb alloy ingot. First, Ti, Zr, and Nb with high melting points are smelted into TiZrNb melt; the power of the arc melting furnace is turned off, and the TiZrNb melt is cooled and solidified to form a TiZrNb alloy ingot. Tur...

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Abstract

The invention discloses a smelting and casting method and a casting device of a titanium-based amorphous composite material. The smelting and casting method has the advantages that the force effect in the electromagnetic induction principle is utilized, alloy in a crucible is suspended in the air for smelting, so that the pollution caused by contact with the crucible is avoided and the control for the alloy heating state is realized; when the smelting process is finished, a heating power supply is switched off, an electromagnetic valve for suction casting or spray casting is opened, so that the rapid mold-filling of alloy solution is realized; in the spray-casting process, the control to the spray-casting speed is realized by changing the level of the air pressure in a gas storage tank, and further the amorphous composite material with different microscopic structures is prepared by controlling the solidification process; the defects in the prior art are overcome, the large-size titanium-based amorphous composite material is obtained by integrating the prior art, the stable control of the process to the organization structure is realized by adjusting process parameters such as temperature, temperature holding time, circular heating times and casting speed, and an ideal optimized design structure is obtained.

Description

technical field [0001] The invention belongs to the technical field of preparation of amorphous composite materials, and in particular provides a melting and casting method for titanium-based amorphous composite materials and a special casting device thereof. Background technique [0002] Due to its special atomic structure of long-range disorder and short-range order, amorphous alloys exhibit more excellent properties than traditional crystalline alloys, such as high strength, high hardness, high corrosion resistance, excellent magnetic properties and certain temperature Superplasticity within the range, etc., has shown great application value in the fields of aerospace devices, precision machinery and information. However, due to the poor room temperature plasticity and small critical size of amorphous alloys, the wide application of amorphous alloys is greatly restricted. The titanium-based amorphous composite material obtained by the autogenous composite method has exce...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C1/03B22D1/00B22D18/06B22D2/00
Inventor 王军寇宏超李金山李力源张铁邦唐斌胡锐薛祥义
Owner NORTHWESTERN POLYTECHNICAL UNIV
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