Environmental-friendly antirust cutting fluid and preparation method thereof

A cutting fluid and weight technology, applied in the field of anti-rust cutting fluid and its preparation, can solve the problems of high oil content, non-compliance with emission standards, and high production cost, and achieve the effects of simple preparation method, clear and bright solution, and low production cost.

Active Publication Date: 2014-08-06
HUBEI UNIV OF EDUCATION
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

But this cutting fluid also has some deficiencies. First, the service life is short, especially in summer when the temperature is high, and the cutting fluid is easy to deteriorate, which makes the workpieces using the cutting fluid rusted; secondly, the sodium nitrite contained in the cutting fluid is harmful to the human body. , and when sodium nitrite is mixed with sodium carbonate, it is easy to produce hard crystals, which will not only adversely affect the quality of the workpiece, but also bring difficulties to equipment maintenance and maintenance; again, from the perspective of environmental protection, this kind of The emulsified ointment in the cutting fluid is made based on engine oil, which has a high oil content, does not meet the environmental protection emission standards, and consumes a lot of energy and high production costs

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] Embodiment 1, in this embodiment 1, anti-rust cutting fluid is prepared according to the following method

[0027] According to the weight of antirust cutting fluid to be synthesized,

[0028] (1) Take 0.5% boric acid by weight and mix it with 4% triethanolamine by weight, heat in an oil bath, stir while heating, control the temperature of the oil bath to 110°C, stop heating after 3 hours, and obtain light yellow and clear solution.

[0029] (2) Take 5% oleic acid by weight, heat and stir in a water bath, and control the temperature of the water bath to 65°C. After the oleic acid is completely dissolved, slowly add 1.2% by weight of triethanolamine and continue to heat and stir. After 45 minutes Turn off heat.

[0030] (3) Take 0.1% by weight of rosin and 0.4% by weight of triethanolamine, mix, heat and stir at 90°C, and stop the reaction after the rosin is completely dissolved.

[0031] (4) Mix the three solutions obtained in steps (1), (2) and (3) evenly, add 0.5% ...

Embodiment 2

[0032] Embodiment 2, in this embodiment 2, anti-rust cutting fluid is prepared according to the following method

[0033] According to the weight of antirust cutting fluid to be synthesized,

[0034] (1) Take 1% boric acid by weight and mix it with 15% triethanolamine by weight, heat in an oil bath, stir while heating, control the temperature of the oil bath to 100°C, stop heating after 3 hours, and obtain light yellow and clear solution.

[0035] (2) Take 2.5% oleic acid by weight, heat and stir in a water bath, and control the temperature of the water bath to 70°C. After the oleic acid is completely dissolved, slowly add 0.8% by weight of triethanolamine and continue to heat and stir. After 45 minutes Turn off heat.

[0036] (3) Take 1% by weight rosin and 2.5% by weight triethanolamine, mix, heat and stir at 90°C, and stop the reaction after the rosin is completely dissolved.

[0037] (4) Mix the three solutions obtained in steps (1), (2) and (3) evenly, add 1% by weight...

Embodiment 3

[0038] Embodiment 3, in this embodiment 3, anti-rust cutting fluid is prepared according to the following method

[0039] According to the weight of antirust cutting fluid to be synthesized,

[0040] (1) Take 2.5% boric acid by weight and mix it with 24% triethanolamine by weight, heat in an oil bath, stir while heating, control the temperature of the oil bath to 100°C, stop heating after 4 hours, and obtain a light yellow and clear solution.

[0041] (2) Take 1% oleic acid by weight, heat and stir in a water bath, and control the temperature of the water bath to 75°C. After the oleic acid is completely dissolved, slowly drop in 0.5% by weight of triethanolamine and continue to heat and stir. After 45 minutes Turn off heat.

[0042] (3) Take 2% rosin by weight and 5% triethanolamine by weight, mix, heat and stir at 90°C, and stop the reaction after the rosin is completely dissolved.

[0043] (4) Mix the three solutions obtained in steps (1), (2) and (3) evenly, add 2% dodec...

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PUM

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Abstract

The invention discloses antirust cutting fluid and a preparation method thereof. The antirust cutting fluid comprises the ingredients in percentage by mass: 0.5-2.5% of boric acid, 4.9-30.2% of triethanolamine, 1-5% of oleic acid, 0.5-2% of dodecyl dimethyl betaine, 0.1-2% of rosin, 0.1-0.5% of defoamer, 1-5% of lubricant and the balance of water. The preparation method comprises the steps of firstly enabling boric acid, oleic acid and rosin, which are in the formula ratio, to respectively react with triethanolamine, then, mixing three solutions which are obtained through reaction, then, adding a proper amount of dodecyl dimethyl betaine, a proper amount of defoamer, a proper amount of lubricant and the balance of water, heating and uniformly stirring. The antirust cutting fluid disclosed by the invention has good rust resistance and lubricating property to first-level cast iron; both original cutting fluid and diluted liquid thereof are stable in performance and low in cost and are harmless to environment and human.

Description

technical field [0001] The invention belongs to the field of fine chemicals, and relates to an environmentally friendly antirust cutting fluid and a preparation method thereof. Background technique [0002] Cutting fluid is an industrial liquid used for cooling and lubricating cutting tools and workpieces during metal cutting, cutting and grinding. It should have good cooling performance, lubricating performance, antirust performance, degreasing and cleaning function, and anti-corrosion function. . [0003] In the machining process, people have long used an emulsified cutting fluid formulated with emulsified ointment, sodium carbonate, and sodium nitrite. But this cutting fluid also has some deficiencies. First, the service life is short, especially in summer when the temperature is high, and the cutting fluid is easy to deteriorate, which makes the workpieces using the cutting fluid rusted; secondly, the sodium nitrite contained in the cutting fluid is harmful to the human...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10M173/02C10N40/22C10N30/12C10N30/06
Inventor 吴田刘琼马晓玲陈功轩
Owner HUBEI UNIV OF EDUCATION
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