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A method for preparing high flatness tungsten-nickel-iron alloy plate

A tungsten-nickel-iron alloy and flatness technology is applied in the field of preparing high-flatness tungsten-nickel-iron alloy plates, which can solve the problems affecting the flatness of finished products, the limitation of total deformation, long production cycle, etc. Small, area-increasing effect

Active Publication Date: 2015-12-23
上海六晶科技股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

There are many problems in these methods. The first problem involved is that the production cycle is too long. Generally, there are 2 to 3 production processes. Taking the production of tungsten-nickel-iron alloy sheets with a thickness of less than 1 mm as an example, the production cycle is at least 2 to 5 days; The second is high energy consumption: hot forging, hot rolling, annealing and other processes must use high-power high-temperature heating furnaces, which consume high energy consumption; third, the yield rate is low, and cracking and scrapping are easily generated during high-temperature processing to produce 1mm thick Take tungsten-nickel-iron alloy thin plate as an example, its comprehensive finished product rate is only about 50%; Fourth, the investment in equipment used is large, and there are many types and quantities, and most of them are processing equipment with high power and large tonnage, which require a large processing site, and tungsten Nickel-iron alloy foil material adopts the method of single sheet feeding and rolling
As the thickness of the material decreases during rolling, the total deformation of the material is limited, and the rolling force of the roll on the sheet during the rolling process is uneven, resulting in a large difference between the same sheet after the sheet is rolled, and the leveling Rolling defects such as double-sided waves, unilateral waves or medium-waves will be generated later, which will directly affect the flatness of the final product.

Method used

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  • A method for preparing high flatness tungsten-nickel-iron alloy plate

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Experimental program
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Effect test

Embodiment 1

[0048] The tungsten-nickel-iron alloy powder after granulation and drying is rolled into a billet, the rolling pressure is controlled at 40KN, and the rolling speed is controlled at 2.5cm / s, and the tungsten-nickel-iron alloy powder is rolled into a thin plate green body with a thickness of 1.8mm .

[0049] The prepared tungsten-nickel-iron alloy thin plate green body is placed in a sintering furnace, and sintered under the protection of hydrogen to obtain a sintered tungsten-nickel-iron alloy thin plate. The sintering temperature is 1300 ° C and the sintering time is 3 hours.

[0050] The sintered body is cold-rolled and rolled, and cold-rolled for several passes until the total deformation of the thin plate reaches 40%.

[0051] Place the cold-rolled tungsten-nickel-iron alloy sheet in a sintering furnace for refiring, the protective atmosphere is hydrogen, the refiring temperature is 1300°C, and the refiring time is 3 hours.

[0052] Repeat the first two steps until the th...

Embodiment 2

[0055] The tungsten-nickel-iron alloy powder after granulation and drying is rolled into a billet, the rolling pressure is controlled at 60KN, and the rolling speed is controlled at 2.0cm / s, and the tungsten-nickel-iron alloy powder is rolled into a thin plate green body with a thickness of 1.6mm .

[0056] The prepared tungsten-nickel-iron alloy thin plate green body is placed in a sintering furnace, and sintered under the protection of hydrogen to obtain a tungsten-nickel-iron alloy thin plate sintered body. The sintering temperature is 1300 ° C and the sintering time is 2.5 hours.

[0057] The sintered body is cold-rolled and rolled, and cold-rolled for several passes until the total deformation of the thin plate reaches 40%.

[0058] Place the cold-rolled tungsten-nickel-iron alloy sheet in a sintering furnace for refiring, the protective atmosphere is hydrogen, the refiring temperature is 1250°C, and the refiring time is 2.5 hours.

[0059] Repeat the first two steps unt...

Embodiment 3

[0062] The tungsten-nickel-iron alloy powder after granulation and drying is rolled into a billet, the rolling pressure is controlled at 80KN, and the rolling speed is controlled at 1.5cm / s, and the tungsten-nickel-iron alloy powder is rolled into a thin plate green body with a thickness of 1.2mm .

[0063] The prepared tungsten-nickel-iron alloy thin plate green body is placed in a sintering furnace, and sintered under the protection of hydrogen to obtain a sintered tungsten-nickel-iron alloy thin plate. The sintering temperature is 1250 ° C and the sintering time is 2.5 hours.

[0064] The sintered body is cold-rolled and rolled, and cold-rolled for several passes until the total deformation of the thin plate reaches 40%.

[0065] Place the cold-rolled tungsten-nickel-iron alloy sheet in a sintering furnace for refiring, the protective atmosphere is hydrogen, the refiring temperature is 1250°C, and the refiring time is 2 hours.

[0066] Repeat the first two steps until the ...

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Abstract

The invention relates to a method for preparing a high-flatness tungsten-nickel-iron alloy plate. The method comprises the following steps of pressing granulated and dried tungsten-nickel-iron alloy powder, and rolling the tungsten-nickel-iron alloy powder to obtain a tungsten-nickel-iron alloy green body with a thickness of 0.5 to 1.8mm and uniform density; placing the obtained tungsten-nickel-iron alloy green body into a sintering furnace, sintering the tungsten-nickel-iron alloy green body under the protection of hydrogen, and cold-rolling the sintered tungsten-nickel-iron alloy green body until the deformation reaches 40 percent; re-sintering the cold-rolled tungsten-nickel-iron alloy green body for 1 to 3 hours at the re-sintering temperature of 1,100 to 1,300 DEG C under the protection of hydrogen; repeating the former two steps until the thickness of the green body is smaller than 0.4mm; overlaying two tungsten-nickel-iron alloy plates with the thickness of 0.15mm, and rolling-milling the tungsten-nickel-iron alloy plates for about 25 times under the pressure of about 15T until the thickness of a single plate is less than 0.1mm. According to the method, a production process is simplified, the energy consumption is lowered, the production cost is reduced, and green production is ensured.

Description

technical field [0001] The invention belongs to the technical field of tungsten-nickel-iron alloy processing, in particular to a method for preparing a high-flatness tungsten-nickel-iron alloy plate. Background technique [0002] High-precision tungsten alloy devices are obtained through precision machining of tungsten-based high-density alloys, which are widely used in the fields of collimators and detectors for medical CT machines. With the development of CT machines, the flatness requirement of collimators has been increased from less than 0.03 to less than 0.02, which poses new challenges to the preparation of tungsten alloy thin materials. [0003] The existing main technologies for processing tungsten-nickel-iron alloy materials include the following: hot forging + cold forging treatment method, hot pressing + repressing finishing treatment method, hot rolling + repressing finishing treatment method, etc. There are many problems in these methods. The first problem inv...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B22F3/18
Inventor 张丽娟朱玉斌
Owner 上海六晶科技股份有限公司
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