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Preparation method of silver tin oxide electric contact materials

An electrical contact material, silver tin oxide technology, is applied in the production of electrical contact materials for low-voltage electrical appliances, and in the field of preparation of silver tin oxide electrical contact materials. The effect of environmental protection pressure and easy control of operation process

Active Publication Date: 2014-10-29
CHENZHOU CITY JINGUI SILVER IND CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In this method, such as Chinese patents CN03113533 and CN201210130542.1, in order to ensure the morphology of metallic silver when it is reduced and precipitated to ensure uniformity, it is necessary to add ammonia water to complex the silver ions. Subsequent water treatment to meet environmental protection requirements brings great pressure, and the dispersion of the chemical components of the materials prepared by this method is not very uniform

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] Take 13.5kg of silver nitrate, 3.4kg of tin nitrate, and 25.5L of distilled water, put them into a 30L reaction tank and stir until the solute is completely dissolved, and prepare an aqueous solution containing silver nitrate and tin nitrate; add 25L of mass to another 30L reaction tank Add 25g of sodium hexametasulfate to an aqueous solution of sodium carbonate with a fraction of 25%, stir until the solute is completely dissolved, and prepare an aqueous solution of sodium carbonate containing a sodium hexametaphosphate dispersant.

[0032] Slowly add the prepared aqueous solution containing silver nitrate and tin nitrate to the sodium carbonate aqueous solution containing sodium hexametaphosphate dispersant, while stirring at a high speed of 750 r / min, and in the aqueous solution containing silver nitrate and tin nitrate After completely pouring into the sodium carbonate aqueous solution containing sodium hexametaphosphate dispersant, keep high-speed stirring within 3 h...

Embodiment 2

[0037]Dissolve 14.5kg of silver nitrate and 2kg of tin nitrate in 25.5L of distilled water in a 30L reaction tank to prepare an aqueous solution containing silver nitrate and tin nitrate; add 25L of sodium carbonate with a mass fraction of 25% to another 30L reaction tank Add 25g of sodium hexametasulfate to the aqueous solution, stir until the solute is completely dissolved, and prepare an aqueous solution of sodium carbonate containing sodium hexametaphosphate dispersant. Under high-speed stirring at 800 r / min, slowly add the aqueous solution containing silver nitrate and tin nitrate to the sodium carbonate aqueous solution containing sodium hexametaphosphate dispersant, and continue stirring for 2.5 hours after the reaction is complete. Then the mixture containing silver carbonate and tin carbonate was vacuum filtered to obtain silver carbonate precipitate and tin carbonate precipitate, and the precipitate was washed twice with distilled water. The washed precipitate was ca...

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PUM

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Abstract

The invention provides a preparation method of silver tin oxide electric contact materials. Firstly, a method for preparing a solution is adopted, an aqueous solution containing silver nitrate and tin nitrate reacts with a sodium carbonate aqueous solution containing a sodium hexametaphosphate dispersing agent, a mixture containing silver carbonate and tine carbonate is obtained under the action of high-speed stirring and the sodium hexametaphosphate dispersing agent, silver tin oxide compound powder with fine particles is obtained through the processing of filtering, forging and mechanical grinding, the preparation of the silver tin oxide electric contact materials uniform in component in the subsequence powder metallurgy process is facilitated, and the preparing process is environmentally friendly. The preparation method of the silver tin oxide electric contact materials is simple and easy to control, short in production cycle, low in pollution, low in cost and favorable for industrial production.

Description

technical field [0001] The invention relates to the field of metal-based composite materials, in particular to a method for preparing an electrical contact material of silver tin oxide, which is mainly used in the production of electrical contact materials for low-voltage electrical appliances. Background technique [0002] Silver tin oxide electrical contact material is a new generation of non-toxic and environmentally friendly electrical contact material replacing silver cadmium oxide contact material. It has excellent anti-welding performance, good resistance to burning loss, high electrical life and environmental protection performance, and is widely used Used in various contactors, relays, circuit breakers and switches. [0003] At present, there are three main methods for preparing silver tin oxide electrical contact materials at home and abroad: powder mixing method, internal oxidation method, and chemical method. The mixed powder method is to mix silver powder and t...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22F9/24B22F3/16B22F3/20H01H1/0237
Inventor 陈兰谢兆凤
Owner CHENZHOU CITY JINGUI SILVER IND CO LTD
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