Preparation method of silver tin oxide electric contact materials
An electrical contact material, silver tin oxide technology, is applied in the production of electrical contact materials for low-voltage electrical appliances, and in the field of preparation of silver tin oxide electrical contact materials. The effect of environmental protection pressure and easy control of operation process
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Embodiment 1
[0031] Take 13.5kg of silver nitrate, 3.4kg of tin nitrate, and 25.5L of distilled water, put them into a 30L reaction tank and stir until the solute is completely dissolved, and prepare an aqueous solution containing silver nitrate and tin nitrate; add 25L of mass to another 30L reaction tank Add 25g of sodium hexametasulfate to an aqueous solution of sodium carbonate with a fraction of 25%, stir until the solute is completely dissolved, and prepare an aqueous solution of sodium carbonate containing a sodium hexametaphosphate dispersant.
[0032] Slowly add the prepared aqueous solution containing silver nitrate and tin nitrate to the sodium carbonate aqueous solution containing sodium hexametaphosphate dispersant, while stirring at a high speed of 750 r / min, and in the aqueous solution containing silver nitrate and tin nitrate After completely pouring into the sodium carbonate aqueous solution containing sodium hexametaphosphate dispersant, keep high-speed stirring within 3 h...
Embodiment 2
[0037]Dissolve 14.5kg of silver nitrate and 2kg of tin nitrate in 25.5L of distilled water in a 30L reaction tank to prepare an aqueous solution containing silver nitrate and tin nitrate; add 25L of sodium carbonate with a mass fraction of 25% to another 30L reaction tank Add 25g of sodium hexametasulfate to the aqueous solution, stir until the solute is completely dissolved, and prepare an aqueous solution of sodium carbonate containing sodium hexametaphosphate dispersant. Under high-speed stirring at 800 r / min, slowly add the aqueous solution containing silver nitrate and tin nitrate to the sodium carbonate aqueous solution containing sodium hexametaphosphate dispersant, and continue stirring for 2.5 hours after the reaction is complete. Then the mixture containing silver carbonate and tin carbonate was vacuum filtered to obtain silver carbonate precipitate and tin carbonate precipitate, and the precipitate was washed twice with distilled water. The washed precipitate was ca...
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