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77results about How to "Solve environmental pressure" patented technology

Method for treating chlorosilane slurry residual liquid

The invention provides a method for retrieving silicon tetrachloride, silicon powder and copper or / and preparing silicate ester by treating chlorosilane slurry residual liquid. The method comprises the following steps: separating chlorosilane slurry residual liquid through solid-liquid separation in step I; directly feeding a liquid phase into a silicon tetrachloride storage tank or purifying silicon tetrachloride in a step III; reacting the solid phase in the step II to lead residual chlorosilane to react and generate silicate ester and hydrogen chloride, and dissolving other chlorides in anorganic solvent; distilling and reclaiming silicate ester from the reacting liquid phase in the step IV, returning the reclaimed hydroxyl-containing solvent and stabilizer to step II for recycling, hydrolyzing and neutralizing kettle bottom solution in the step V; and adding an alkaline liquor, reacting metal chloride to generate hydroxide precipitate, directly removing the Three Wastes from the neutralized reacting liquid phase in the step VII, extracting copper from the hydroxide precipitate through the step VI, and further treating in the step VIII to obtain metal copper; and treating the solid, which is copper-containing silicon powder, obtained in the step II to reclaim silicon powder and copper after step VI and step VIII treatment.
Owner:四川绿源聚能环保科技有限责任公司

Device system for treating chlorosilane slag slurry raffinate

InactiveCN107539991ADoes not introduce secondary pollutionSolve resource problemsSilicon organic compoundsSiliconSlagSlurry
The invention provides a device system for treating chlorosilane slag slurry raffinate to recycle silicon tetrachloride, silicon powder, copper or / and preparing silicate ester. The chlorosilane slag slurry raffinate is added into a solid-liquid separation device I; after separation, a liquid phase directly flows into a silicon tetrachloride storage tank or a silicon tetrachloride purification device III, and a solid phase is discharged into a reaction device II, so that residual chlorosilane and an organic solvent react to generate the silicate ester and hydrogen chloride, and other chloridesare dissolved into the organic solvent; after the solid-liquid separation, the liquid phase is distilled by a device IV, so that the silicate ester is separated out; an extracted material at the top of a tower returns into the reaction device II, and kettle base solution flows into a hydrolysis and neutralization device V; alkali liquor is added into the device V and is in reaction with the metalchlorides to generate a hydroxide precipitate and chlorate solution, a liquid phase flows into a three wastes treatment device VII, a solid phase is transferred to a copper extraction device VI for copper extraction, and copper is further treated by a device VIII, so as to obtain recovery copper; a solid phase in the device II is copper-contained silicon powder and is treated by the device VI andthe device VIII, so as to recovery silicon powder and copper.
Owner:四川绿源聚能环保科技有限责任公司

Reusable modified guar gum fracturing fluid system

The invention relates to a reusable modified guar gum fracturing fluid system. According to the technical scheme, the system comprises a primary mixed solution and a secondary mixed solution, wherein chemicals of a reusable fracturing system are adopted as the primary mixed solution and include compound modified guar gum, an organo-boron cross-linking agent, a low-temperature activator, a cleanup activator, a gel breaker removal adhesion preserving agent, an ionic equilibrium regulator, a molecular remodeling carding agent and a gel breaker. The base fluid formula of the secondary mixed solution includes an antibacterial agent formaldehyde, a gel breaker removal adhesion preserving agent, an ionic equilibrium regulator, thickening agent guar gum and a cleanup activator. The system has the advantages that the problems about water lack and environmental protection pressure during oilfield development in dry and rainless regions are solved, and secondary utilization of flowback fluid of fracturing fluid is achieved. On the premise that the requirements for safe fracturing construction and reservoir protection are met, fracturing fluid is easy to maintain and process and can be repeatedly used, the treatment amount of the flowback fluid is reduced, and water resources are saved.
Owner:DONGYING SPRING PETROLEUM ENG TECH

Waste water heat energy utilization method applicable to viscose staple fiber industry

The invention discloses a waste water heat energy utilization method applicable to the viscose staple fiber industry. The waste water heat energy utilization method applicable to the viscose staple fiber industry comprises processes of performing heat exchange and recycling on waste hot water during viscose staple fiber production, wherein the waste hot water comprises plasticizing tank overflow water; the processes comprise utilizing the plasticizing tank overflow water to perform step-by-step heat exchange sequentially on plasticizing tank make-up water, desulfurizing liquid and packaged cooling water, the packaged cooling water is conveyed to a cutting machine after heat exchange is performed, and then utilized by a refiner to obtain green cut water, and the green cut water returns to the cutting machine or is conveyed to a plasticizing tank water supplementing tank to serve as plasticizing tank supplement water. The waste water heat energy utilization method applicable to the viscose staple fiber industry achieves comprehensive recycling and utilization of various types of waste hot water and meanwhile achieves heat exchange treatment on specific mediums requiring heating during the viscose staple fiber production, thereby making full use of waste heat of the waste hot water, promoting energy conservation and consumption reduction for enterprises on the basis of existing process waste water treatment and under the premise of no flow losses, and obtaining high social benefits and economic benefits.
Owner:YIBIN GRACE +2

Equipment and method for crushing and sorting solar cell components

The invention provides an equipment and method for crushing and sorting solar cell components. The equipment for crushing and sorting the solar cell components comprises a hammering and splitting device, a winnowing separation device, a vibratory screening device, an electrostatic sorting device and an airflow crushing and grading device. A physical environmental protection method is adopted. Thesolar cell components, which remove aluminum frames and glass, are hammered into particle mixtures by the hammering and splitting device, and plastic particles are screened for recycling and meanwhilecopper materials such as metal solder strip particles and metal bus bar particles are screened and recycled in advance. The remaining particle mixtures are crushed into powder through the airflow crushing and grading device, so that the separation and sorting of silicon, silver, aluminum and other elements in cells is realized. The equipment has high processing speed, can automatically realize environmentally-friendly recycling of waste solar cell components, especially crystal silicon components on a larger scale, and solves the problems of environmental pressure and resource reuse caused bylarge-scale decommissioning of the solar cell components are solved.
Owner:HEBEI UNIVERSITY

Preparation method of (S)-1-(2-chloracetyl)pyrrolidine-2-carbonitrile

The invention discloses a preparation method of (S)-1-(2-chloracetyl)pyrrolidine-2-carbonitrile, which is applied to the field of chemical synthesis. The preparation method comprises the following steps of (1) dropwise adding chloracetyl chloride into a mixed solution composed of L-prolinamide, organic alkali and dichloromethane, and reacting after finishing the dropwise adding operation to obtain a reaction solution I containing 1-chloroacetylpyrrolidine-2-carboxamide; and (2) enabling the reaction solution I to react with phosphorus oxychloride serving as a dehydrating agent to obtain (S)-1-(2-chloracetyl)pyrrolidine-2-carbonitrile. In the step (1), the temperature of the mixed solution I composed of L-prolinamide, organic alkali and dichloromethane ranges from 10 DEG C below zero to 60 DEG C, the temperature of reaction carried out after the dropwise adding operation is finished ranges from 50 DEG C below zero to 10 DEG C below zero, the reaction carried out after the dropwise adding operation is finished lasts for 0.5-4h, and the molar ratio of L-prolinamide to chloracetyl chloride is 1:(1.05-1.31). The preparation method is short in reaction step and simple in operation and has the advantages that the raw material cost is low, the yield is high, the product quality is good, little environment pollution can be caused, green resources can be favorably protected, the required equipment is simple, and the dosage of the used organic solvent is low.
Owner:NORTHEAST PHARMA GRP

Method for preparing high-purity lithium fluoride

The invention discloses a method for preparing high-purity lithium fluoride, comprising the following steps of 1) sufficiently mixing lithium carbonate powder and hydrochloric acid for reaction to obtain a lithium chloride solution with the pH value of 6 to 7; 2) adding excessive hydrofluoric acid solutin into the lithium chloride solution obtained in the step 1) for sufficient mixing, and reacting to obtain a mixed solution containing lithium fluoride precipitate; 3) standing the mixed solution obtained in the step 2) and filtering to obtain a lithium fluoride wet solid and hydrochloric acidmother liquor; 4) washing and performing vacuum drying on the lithium fluoride wet solid obtained in the step 3) to obtain the high-purity lithium fluoride solid. According to the method provided by the invention, cheap and available hydrochloric acid is taken as an intermediate raw material for preparing lithium fluoride, lithium chloride with good water solubility is firstly prepared using hydrochloric acid and lithium carbonate, then lithium chloride is reacted with hydrogen fluoride to obtain lithium fluoride and the hydrochloric acid mother liquor, and the hydrochloric acid solution withlithium fluoride separated out is recycled to be reacted with lithium carbonate; the method has the advantages that the raw material cost is low, the process is simple, and the product conversion rateis high.
Owner:GUIZHOU INST OF TECH +1

Fireproof protection and decoration integrated structure on steel member

The invention discloses a fireproof protection and decoration integrated structure on a steel member. The fireproof protection and decoration integrated structure comprises the steel member, a steel structure interface mortar layer, a steel wire mesh and a wall spraying mortar layer, wherein the steel member is a bearing structure of a steel structure building; the steel structure interface mortarlayer is applied to the surface of a to-be-sprayed wall spraying mortar layer of the steel member; the steel wire mesh is laid on the surface of the steel structure interface mortar layer; the wall spraying mortar layer is sprayed to the surface of the steel wire mesh and wraps the steel member, the steel structure interface mortar layer and the steel wire mesh completely, and a fireproof protection and decoration integrated layer is formed. Compared with the traditional wrapping and decoration for the steel member through fireproof paint and a light-gauge steel joist system, the novel wall spraying mortar structure for the steel member has the advantages that the system is excellent in fireproof performance, good in overall performance and free of hollowing and cracking, the wall is light in mass, dense, fireproof, sound-insulating, heat-insulating, comfortable, simple and fast to construct, high in practicability and easy to popularize and use, and a construction environment is clean and tidy.
Owner:SHANGHAI KENAI NEW MATERIAL TECH CO LTD

Method for treating steel slag

The invention relates to a method for treating steel slag, and belongs to the technical field of steel slag treatment. The method comprises the following steps that 1, liquid-state converter steel slag is discharged, and operation of slag splashing for converter protection is conducted; 2, reduction smelting is conducted on the liquid-state steel slag obtained in the step 1, slag discharging is conducted, reduced slag is obtained, iron discharging is conducted, reduced molten iron is obtained, and the reduced slag is recycled; 3, the reduced molten iron obtained in the step 2 is subjected to desulfuration and / or desilicication and / or dephosphorization operation, purified molten iron and slag are obtained, and the purified molten iron is smelted and then recycled; 4, the slag obtained in the step 3 is cooled with water and then filtered, filtrate and filter residues are obtained, and the filter residues are dried, smelted and recycled; 5, acid is added into the filtrate obtained in thestep 4 till the PH is neutral, precipitates and gas are produced, the precipitates are filtered and recycled, and filtrate obtained through filtering is retained for use; and 6, the gas and the filtrate which are obtained in the step 5 are treated through a FeCl3 solution. The method for treating the steel slag has the characteristics of being high in efficiency and environmentally friendly.
Owner:SHOUGANG JINGTANG IRON & STEEL CO LTD

Device and method for crushing and sorting solar cell modules

The invention provides a device and a method for crushing and sorting solar cell modules. The device comprises a shearing device, a grinding device, a winnowing separation device, a vibration screening device and an airflow crushing and grading device. According to the device and the method for crushing and sorting the solar cell modules, a physical environment-friendly method is adopted, the solar cell modules with aluminum frames and the glass removed are cut into fragments through the shearing device, the fragments are ground into a particle mixture through the grinding device, and then plastic particles in the particle mixture are sorted out and collected through the winnowing separation device and the vibration screening device. Battery piece particles are crushed into powder throughthe airflow crushing and grading device, separation and sorting of silicon, silver, aluminum, copper and other elements in battery pieces are achieved, the separation purity of the silicon, silver, aluminum, copper and other elements is high, the treatment speed is high, environment-friendly recycling of waste solar cell modules, especially crystalline silicon modules, can be automatically achieved on a large scale, and the problem of environmental pressure and resource reutilization caused by large-scale retirement of the solar cell modules is solved.
Owner:HEBEI UNIVERSITY

Dry kiln interior desulfurizer for smelting ferronickel through RKEF method

The invention discloses a dry kiln interior desulfurizer for smelting ferronickel through an RKEF method. The dry kiln interior desulfurizer comprises a cylinder internally provided with a lifting board. The cylinder is oblique, and the front end of the cylinder is lower than the rear end of the cylinder. An air inlet and an air outlet are formed in the front end and the rear end of the cylinder.The front end and the rear end of the cylinder are rotationally connected with a kiln head cover and a kiln tail cover correspondingly. A feeding pipe is arranged on the top of the kiln head cover, and an ash unloading hopper is arranged at the bottom of the kiln head cover. A discharging hopper is arranged on the kiln tail cover. Rolling rings are arranged at the front portion and the rear portion of the cylinder correspondingly and rotationally connected with supporting wheels. A rotation tooth disk is arranged at the outer diameter position of the middle portion of the cylinder. Materials enter the cylinder from the position of the feeding pipe, a desulfurizing agent and sulfur oxides are subjected to the sufficient reaction till the purpose of desulfuration is achieved, and desulfurized materials are discharged out of the position of the discharging hopper. The lifting board in the cylinder sufficiently raises materials, and the reaction effect is improved. Purified gas enters thecylinder from the position of the air inlet, high-temperature heat is provided for the interior of the cylinder, and the material drying and desulfuration effects are promoted.
Owner:临沂鑫海新型材料有限公司

Steel slag selecting method

The invention discloses a steel slag selecting method. The steel slag selecting method is characterized by comprising the following steps that S1, primary magnetic separation is carried out after steel slag is subjected to primary ball milling until the particle size of the steel slag is 80-100 meshes, and a primary magnetic separation concentrate and tailings are obtained for later use; S2, demagnetic treatment is carried out on the primary magnetic separation concentrate, secondary ball milling is carried out on the demagnetized primary magnetic separation concentrate until the particle sizeis 180-200 meshes, and secondary magnetic separation is carried out on the concentrate subjected to ball milling to obtain secondary magnetic separation concentrate and tailings for later use; and S3, demagnetic treatment is carried out on the secondary magnetic separation concentrate, then three-section ball milling and multiple times of magnetic separation and reselection treatment are carriedout on the demagnetized concentrate to obtain an ultrahigh-purity magnetite concentrate and a high-grade iron ore concentrate. The steel slag selecting method is mainly used for selecting the ultrahigh-purity magnetite concentrate from the steel slag, belongs to a pure physical method, does not use a chemical agent in the production process, and is green and environment-friendly; and the production cost is 35% of the production cost of a traditional chemical method for producing the ultrahigh-purity magnetite concentrate, and the method has remarkable economic benefits and market popularization values.
Owner:周涛 +2

Hyaluronic acid-glucosamine grafted copolymer, and preparation method and application thereof

PendingCN111732675AReduce releaseCan maintain long-acting mechanism of actionOrganic active ingredientsSkeletal disorderArticular cavityLong chain
The invention discloses a hyaluronic acid-glucosamine grafted copolymer, and a preparation method and application thereof. The preparation method of the hyaluronic acid-glucosamine grafted copolymer comprises the following steps: mixing a condensing agent, glucosamine or salt thereof and water to obtain a mixed solution; adjusting the pH value of the mixed solution, then adding hyaluronic acid orsalt thereof, and performing an amidation reaction to obtain the hyaluronic acid-glucosamine grafted copolymer. The preparation method is simple and efficient; the method is performed in an aqueous solution to avoid environmental protection pressure caused by using an organic solvent; reaction conditions are mild, so long chains and molecular structures of hyaluronic acid or salt thereof in a reaction system cannot be damaged, and high molecular weight can be maintained; and through mediation of the condensing agent, hyaluronic acid and glucosamine are connected through a stable covalent bond,so the obtained hyaluronic acid-glucosamine grafted copolymer is injected into an articular cavity to directly recover the viscoelasticity of synovial fluid, and the hyaluronic acid-glucosamine grafted copolymer has the effects of lubricating and nourishing joints and has slow absorptivity.
Owner:SHANDONG BLOOMAGE HYINC BIOPHARM CORP LTD

Internal pre-reduction desulfurization device for rotary kiln during ferronickel smelting by virtue of RKEF process

The invention discloses a pre-reduction desulfurization device in a rotary kiln for smelting ferronickel by the RKEF method, which comprises a block-shaped bin with a quantitative feeding conveyor belt below; The outlet of the vertical mill is connected with the inlet of the upper part of the powder collector; the bottom of the powder collector is connected with the feeding pipe; the outlet at the end of the feeding pipe corresponds to the inlet of the top of the finished product warehouse; It is connected with the feed port of the quantitative feeder; one end of the quantitative feeder is connected with the Roots blower, and the other end is connected with the material nozzle; the material nozzle is connected with the rotary kiln. The desulfurizer and reducing agent are ground and transported together and finally blown to the inside of the rotary kiln. They react while the burner sprays flames into the rotary kiln. Pre-reduction desulfurization is carried out in the environment of high temperature and water vapor, and desulfurization can be carried out in the kiln. treatment, which reduces the load of subsequent purification, and at the same time can significantly improve the purification effect, and the emission indicators have been qualitatively improved.
Owner:临沂鑫海新型材料有限公司
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