Preparation method of hollow polyimide fiber membrane applied to sulfide adsorption
A polyimide, fiber membrane technology, applied in chemical instruments and methods, alkali metal compounds, alkali metal oxides/hydroxides, etc., can solve problems such as no adsorption effect of sulfides, no reports yet, and achieve cost Low cost, simple operation and simple preparation process
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Embodiment 1
[0019] (1) Preparation of spinning dope:
[0020] The polyimide matrix material was synthesized from two monomers, pyromellitic dianhydride and 4,4'-diaminodiphenyl ether. Before synthesis, the two monomer raw materials of pyromellitic dianhydride and 4,4'-diaminodiphenyl ether were put into a vacuum drying oven at 120°C for 24 hours, and the solvent N-methylpyrrolidone was removed with activated 3A molecular sieves. Water treatment, the treatment time is more than 24 hours. Take the dried 4,4'-diaminodiphenyl ether (6.01g, 30mmol) and dissolve it in N-methylpyrrolidone (69ml). After the 4,4'-diaminodiphenyl ether is completely dissolved, add Tetracarboxylic dianhydride (6.54 g, 30 mmol). After stirring and reacting at room temperature for 4 hours, a polyamic acid solution with a concentration of 15% by mass was obtained. Then add 9.3g of AgY molecular sieve, the mass percentage of molecular sieve is 10%, fully stir for more than 4 hours, and finally go through vacuum defoa...
Embodiment 2
[0026] (1) Preparation of spinning dope:
[0027] The polyimide matrix material was synthesized from two monomers, pyromellitic dianhydride and 4,4'-diaminodiphenyl ether. Before synthesis, the two monomer raw materials of pyromellitic dianhydride and 4,4'-diaminodiphenyl ether were put into a vacuum drying oven at 120°C for 24 hours, and the solvent N-methylpyrrolidone was removed with activated 3A molecular sieves. Water treatment, the treatment time is more than 24 hours. Take the dried 4,4'-diaminodiphenyl ether (6.01g, 30mmol) and dissolve it in N-methylpyrrolidone (49ml). After the 4,4'-diaminodiphenyl ether is completely dissolved, add Tetraformic dianhydride (6.54g, 30mmol) (note: add in several times, at least 3 times, to ensure full reaction of the monomer). After stirring and reacting at room temperature for 4 hours, a polyamic acid solution with a concentration of 20% by mass was obtained. Afterwards, 11.1 g of AgY molecular sieves were added, the mass percentag...
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