Device for preparing magnesium oxide by saturated brine spray pyrolysis

A technology of spray pyrolysis and magnesium oxide, applied in magnesium oxide and other directions, can solve the problems of producing a large amount of carbon dioxide, complicated process and equipment, and high impurity content in the product, and achieve the effect of improving combustion efficiency, increasing residence time and good product performance.

Active Publication Date: 2014-12-10
EAST CHINA UNIV OF SCI & TECH
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Problems solved by technology

[0005] At present, the traditional method of preparing magnesium oxide in my country is mainly the calcination method of solid ore magnesite. This method has simple process and low cost, but the product has high impurity content and is difficult to remove, and will produce a large amount of carbon dioxide, polluting the environment.
The preparation of magnesium oxide from salt lake brine is mainly through precipitation methods such as ammonium bicarbonate method and milk of lime method. The process and equipment are complicated and the cost is high.

Method used

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  • Device for preparing magnesium oxide by saturated brine spray pyrolysis

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Embodiment 1

[0030] Such as figure 1 As shown, a device that can quickly pyrolyze brine to produce magnesium oxide mainly includes a pyrolysis furnace 1, a hot air system, a feeding system, and a tail gas treatment system.

[0031] There is a discharge port 11 at the bottom of the pyrolysis furnace 1, and four openings at the top, which are: feed port 12, temperature control instrument detection port 13, temperature measurement port 14, and gas outlet 15. There are three combustion gun inlets inside The first combustion gun 26-1, the second combustion gun 26-2, the third combustion gun 26-3 and the flame detector 25; the discharge port 11 is connected with the product bin 17 through the valve 16, and the feed port is installed at 12 places A liquid atomizing nozzle 33 is installed, the nozzle 33 is connected with the feed pump 32, and then connected with the raw material storage tank 31; the temperature control instrument detection port 13 and the temperature measurement port 14 are equipp...

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Abstract

The invention relates to a device for preparing magnesium oxide by saturated brine spray pyrolysis, which comprises a pyrolyzing furnace, a hot-air system and a feed system, wherein the pyrolyzing furnace is a self-made brick / silicon carbide hearth mixed structure; the hot-air system comprises an air compressor, a liquefied petroleum gas tank, a controller, an air liquefied gas premixing pipe, combustion fire lances, an igniter and an instrument system; the feed system is composed of a storage tank, a diaphragm pump, a pipeline and a sprayer; the upper part of the cone is provided with the combustion fire lances (every two combustion fire lances form a 120-degree angle) and additionally provided with a flame detector; the coal gas enters the premixing pipe to be mixed with air under the control of a solenoid valve, and is combusted at the outlets of the combustion fire lances so as to supply heat; the bottom of the whole device is provided with a discharge port, and the top is provided with four openings; and the discharged substance is subjected to dust removal by a ceramic filter and directly absorbed by the saturated alkali solution, thereby producing no environmental pollution. The device can generate the magnesium oxide product by direct spray pyrolysis of saturated brine, and has the advantages of simple technical process, low input cost and favorable product performance.

Description

【Technical field】 [0001] The invention relates to the technical field of inorganic chemical industry. Specifically, it relates to a device for preparing magnesium oxide by spray pyrolysis of saturated brine. 【Background technique】 [0002] Magnesium oxide is an inorganic chemical product with important industrial uses among magnesium salt products. It is widely used in the fields of catalysis, ceramics, plastics and rubber. [0003] Qinghai Chaerhan Salt Lake, located in the central and eastern part of the Qaidam Basin in my country, has more than 3 billion tons of magnesium chloride reserves, ranking first in the country and accounting for 74% of the country's magnesium salt resources. The development and utilization of potassium resources in Chaerhan Salt Lake has produced a large amount of magnesium chloride as a by-product. The annual discharge of old brine containing 33% of magnesium chloride has reached 64 million cubic meters, and the content of chloromagnesite has e...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01F5/10
Inventor 路贵民刘富舟杜玮刘源涛孙泽于建国
Owner EAST CHINA UNIV OF SCI & TECH
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