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Method for producing refined sugar through ion-exchange fiber high efficiency decolorization one-step method

An ion-exchange fiber and fiber-exchange technology, which is applied in the field of high-efficiency decolorization of ion-exchange fibers to produce refined sugar by one-step method, can solve the problem that the ion-exchange resin method cannot meet the requirements of clear juice in cane sugar factories, is rarely used in sugar factories, and has a slow adsorption and exchange rate. and other problems, to achieve the effect of saving the secondary evaporation crystallization process, ensuring the thoroughness of regeneration, and saving energy consumption

Inactive Publication Date: 2014-12-10
桂林正翰科技开发有限责任公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0010] The clarified sugar juice needs to be decolorized and refined. The traditional method is to use bone charcoal, which has good decolorization and ash removal efficiency, but the investment cost of equipment (especially regeneration equipment) is large, and new sugar factories are rarely used.
After the 1970s, granular activated carbon and ion exchange resins were widely used to remove pigment and ash more thoroughly. They can be regenerated but the cost is high. Some sugar factories also use powdered activated carbon.
The shortcomings of this method exposed in use are that non-sugar substances are introduced into the sugar juice, so that the quality of the syrup and the final sucrose crystals will be affected by the addition of reagents that make the syrup alkaline, and sulfur will be present in the sucrose. residues in crystals
[0019] Although ion exchange resins have been widely used in the decolorization process of syrup, there are still obvious disadvantages. The main reason is that ion exchange resins have a macroporous structure, and their decolorization principle belongs to intra-pore exchange. Difficult to wash
At the same time, due to the slow adsorption and exchange speed of the resin, the investment in exchange equipment will be increased in the large-flow sugar production process
In addition, the regeneration of the exchange resin is slow, and the waste liquid after regeneration is difficult to recycle, causing pollution to the environment
Therefore, the ion exchange resin method still cannot meet the requirements of clear juice in sugarcane sugar factories.

Method used

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  • Method for producing refined sugar through ion-exchange fiber high efficiency decolorization one-step method
  • Method for producing refined sugar through ion-exchange fiber high efficiency decolorization one-step method
  • Method for producing refined sugar through ion-exchange fiber high efficiency decolorization one-step method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0079] Decolorization Test of Ion Exchange Fiber on Yaffa Juice

[0080] The test selects the clean juice and clarified juice of the sulfite sugar factory to carry out the static decolorization comparison test. The test results are shown in figure 2 . From figure 2 It can be seen that the decolorization rate of ion exchange fiber to clarified juice is significantly higher than that of clean juice. Clean juice is mixed with clarified juice and filtered juice. Clean juice contains more suspended matter than clarified juice, and suspended matter is easy to cover on the fiber. The surface of the surface, while the ion exchange process is carried out on the surface, the suspended matter prevents the ion exchange and adsorption decolorization process, so that the decolorization efficiency of the clarified juice is reduced. Therefore, the use of ion exchange fibers to decolorize sugar juice should try to avoid the pollution of suspended solids, especially colloids.

Embodiment 2

[0082] Decolorization Test of Ion Exchange Fiber on Sugar Juice by Carbon Method

[0083] The comparison test of the decolorization effect of anion exchange fiber on various sugar juices by carbon method, the results are shown in Table 1.

[0084] Table 1

[0085]

[0086] The test results show that the decolorization effect on Erqing juice is obvious, and the treatment capacity is large.

Embodiment 3

[0088] Effect of Temperature on Decolorization Efficiency of Erqing Juice

[0089] Take 20g of fiber (wet), adjust the temperature of the clear juice by cooling or heating, and measure its color value after reacting for 30 minutes. The results are shown in image 3 .

[0090] From image 3 It can be seen that the optimum temperature range for decolorization of sugar juice by ion exchange fibers is between 65 and 80°C, and above 80°C, the decolorization rate decreases slightly with the increase of temperature, which is because the decolorization process belongs to adsorption. The exchange process belongs to chemical adsorption. The active point on the surface of the ion exchange fiber is chemically combined with the solute, resulting in electron transfer phenomenon. The adsorption exchange process is mainly an exothermic reaction. The temperature has a certain influence on the exchange process, and it is stronger when the temperature is low. It is weaker when the temperature ...

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Abstract

The invention provides a method for preparing refined sugar through an ion-exchange fiber high efficiency decolorization one-step method. The method comprises the following steps: (1) conducting pre-treatment on sugar juice obtained through sugar preparation by a sulfurous acid method and a carbonic acid method; (2) conducting negative-positive-negative three-stage pillar exchange decolorization by adopting ion-exchange fiber until the sugar juice reaches the requirements of a refined sugar clear juice, and collecting into a clear juice box; (3) unloading sugar; (4) evaporating the refined sugar clear juice; (5) boiling sugar; (6) conducting help-crystallization and purging. According to the method provided by the invention, on the basis of the conventional sugar preparation process, the ionic fiber exchange process is added, the two-step method is replaced by the one-step method, and the refined sugar is prepared by directly using the sugar juice obtained through sugar preparation by the sulfurous acid method and the carbonic acid method, so that the technology is simple, the quality index of the sugar juice is improved, the product quality is good, the energy is saved, and the environmental pollution is reduced.

Description

technical field [0001] The invention relates to sugar production, in particular to the production technology of refined sugar, more specifically to a method for producing refined sugar in one-step efficient decolorization of ion exchange fiber. Background technique [0002] With the improvement of people's living standards, people have put forward higher requirements for the quality of white sugar, and the technology of refined sugar has been gradually developed. The existing refined sugar process uses a two-step method, that is, raw sugar is first made, and after the raw sugar is redissolved, it is decolorized by active carbon and ion exchange resin to make refined syrup, and then crystallized into refined sugar. The disadvantage of this process is the need for secondary crystallization, increased steam consumption, and increased energy consumption; the traditional sulfitic and carbonic acid methods can only cook farmland white sugar, and the quality can reach the standard ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C13B20/14
Inventor 郑斌冯长根曾庆轩黄健泉周定怀郑波梁建斌
Owner 桂林正翰科技开发有限责任公司
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