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A producing process for preparing cerium oxide polishing powder

A production process and cerium oxide technology are applied in the production process field of preparing cerium oxide polishing powder, which can solve the problems of high cost of raw materials, waste of energy resources, short service life, etc. quick effect

Inactive Publication Date: 2015-01-07
ZHENGZHOU PUMING NEW MATERIAL
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, China's high-performance polishing powder mainly relies on imports, and the production process of polishing powder is relatively backward. , in which the calcination process is through heating, 1000°C-1080°C calcination heat preservation, cooling, crushing and grading, adding additives, and obtaining finished products; the disadvantage is: the cost of raw materials is high, and more precious and scarce praseodymium is required in addition to the rare earth element lanthanum cerium Neodymium element; polluting the environment, fluorine and other environmentally unfavorable elements are discharged during production and use; waste of energy resources, such as wasting a lot of water resources in the fluorination process, especially in the calcination process, the calcination temperature is high and the process is long , heating, heat preservation, and cooling all require a lot of energy; the polishing powder produced by the existing technology cannot polish hard glass, and it cannot be polished; the service life is not long; at the same time, the polishing efficiency, both the cutting rate and the polishing quality, cannot meet the current domestic demand.

Method used

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  • A producing process for preparing cerium oxide polishing powder

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Effect test

Embodiment 1

[0038] With a purity of 99.95%, a particle size of 8-20μm, and a bulk density of 1.00-1.40g / cm 3 Cerium oxide is used as the raw material. After 120 minutes in the kiln, it is raised to 650°C and held for 80 minutes; then after 90 minutes, it is raised to 950°C and held for 150 minutes; the cerium oxide is quickly poured into cooling water at a temperature of 25°C, and it takes 0.5 min, complete quenching and calcination; dehydration and drying until the moisture content is less than 0.1%; crushing and grading to control the particle size from 2.4 μm to 2.6 μm; adding 0.4% polyethylene glycol 2000 by weight of polishing powder as a dispersant; packaging the finished product.

Embodiment 2

[0040] Using cerium carbonate with a purity of 99.95% as the raw material, heat it up to 650°C in the kiln for 180 minutes, and keep it for 120 minutes; In water, it took 0.5min to complete quenching and calcination; dehydration and drying until the moisture content was less than 0.1%; crushing and grading to control the particle size of 2.4μm-2.6μm; adding 0.5% of the weight of polishing powder polyethylene glycol 2000 as a dispersant; packaging the finished product.

Embodiment 3

[0042] Using cerium oxalate with a purity of 99.95% as the raw material, heat it to 650°C in the kiln for 110 minutes, and keep it for 90 minutes; In water, it took 0.5min to complete quenching and calcination; dehydration and drying until the moisture content was less than 0.1%; crushing and grading to control the particle size of 2.4μm-2.6μm; adding 0.7% of the weight of polishing powder polyethylene glycol 2000 as a dispersant; packaging the finished product.

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Abstract

The invention relates to the technical field of chemical production and particularly relates to a producing process for preparing cerium oxide polishing powder. Producing processes at present for cerium oxide polishing powder have disadvantages that: the environment is polluted; energy resources are wasted; and the polishing efficiency namely the cutting rate, polishing quality and service lifetime of the obtained cerium oxide polishing powder by the processes at present fail to meet requirements. The producing process adopts high-purity cerium oxide or cerous carbonate or cerous oxalate as a raw material, and by steps of heating, maintaining the temperature, performing secondary heating, performing secondary temperature maintaining, quenching, calcinating, removing water, drying, smashing and grading to obtain the polishing powder. A product of the producing process has advantages of high polishing speed, long service lifetime, good polishing quality, simple process, low raw material cost, energy conservation and environment protection.

Description

technical field [0001] The invention relates to the technical field of chemical production, in particular to a production process for preparing cerium oxide polishing powder. Background technique [0002] The application fields of rare earth polishing materials are constantly changing, from traditional TV picture tube glass bulb polishing, rhinestone polishing, etc. to high-performance polishing fields such as liquid crystal display more precise optical instruments and devices. From the perspective of development trend, the field of liquid crystal display and high-grade optical glass processing is the development direction of the application of rare earth polishing materials. High-grade polishing powder has high added value and high profit, and is closely related to the high-tech field with rapid development, so it has broad application prospects. At present, the development and production of high-performance rare earth polishing materials are mainly concentrated in Japan,...

Claims

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Application Information

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IPC IPC(8): C01F17/00C09G1/02C09K3/14
Inventor 程相山周振甫周柯羽姜淑凤王常亮
Owner ZHENGZHOU PUMING NEW MATERIAL
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